Cellulose Nanofiber Dispersion Evaluation via Color Contrast

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Solution Overview

Problem

Cellulose nanofiber dispersions are challenging to evaluate for agglomerates due to their high transparency, making visual identification impossible.

Innovation Solution

A method involving the preparation of cellulose nanofiber dispersions, addition of a colored pigment, and observation with a light microscope to determine the CNF dispersion index, which classifies agglomerates and calculates a dispersion index to assess dispersity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If CNFs are used in a dispersed state in water, then they can be applied for various purposes (reinforcing materials, viscosity maintenance, etc.), but agglomerates form in the dispersion which cannot be visually identified due to high transparency

Engineering Contradiction:
Improveapplication purposesVSAvoidvisual identification of agglomerates
Core Design Contradiction:
Adaptability or versatilityVSDifficulty of detecting and measuring

Solution Approach 1:

The patent applies color change principle by adding a color material to the CNF dispersion. The color material absorbs light and provides contrast, making the transparent agglomerates visible under a microscope. This allows for easy visual detection and evaluation of agglomerate formation without affecting the fundamental properties of the CNF dispersion for its various applications.

Inventive Principle:
Principle #32Color changes

2Measurement precision

If a color material is added to make agglomerates visible, then agglomerates can be detected with a light microscope, but the complexity of the evaluation process increases

Engineering Contradiction:
Improveagglomerate detectionVSAvoidevaluation process
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The color material acts as an intermediary substance that facilitates the detection of agglomerates. It is added to the CNF dispersion to provide optical contrast, enabling visual detection with a standard light microscope. This intermediary approach simplifies the overall evaluation process by making agglomerates visible without requiring complex imaging equipment or sophisticated analysis methods.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables effective evaluation of agglomerates in cellulose nanofiber dispersions, improving dispersity assessment and application reliability in food, cosmetics, and rubber compositions.

Implementation Method 1

adding a color material into the cellulose nanofiber dispersion... observing the cellulose nanofiber dispersion to which the color material has been added with a light microscope

Methodology Applied
Scientific EffectLight absorption: Absorption (EM radiation)

Data Source

PatentUS11092587B2Method for evaluating cellulose nanofiber dispersion
Publication Date: 2021.08.17 NIPPON PAPER IND CO LTD
  • US11092587B2 patent drawing
  • US11092587B2 patent drawing
  • US11092587B2 patent drawing

AI summary

Herein provided are methods for evaluating cellulose nanofiber dispersions, comprising the steps of: (1) preparing a cellulose nanofiber dispersion; (2) adding a color material into the cellulose nanofiber dispersion; and (3) observing the cellulose nanofiber dispersion to which a colored pigment has been added with a light microscope. The methods allow for easy evaluation of whether or not agglomerates of cellulose nanofibers exist in cellulose nanofiber dispersions, which cannot be visually determined.