Co-Carbide Composite Coating for High-Temperature Transfer Rollers

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Solution Overview

Problem

Existing high-temperature material transferring members face issues with build-up resistance, wear resistance, and oxidation resistance, particularly in high-temperature gas atmospheres above 1100°C, leading to indentation defects and reduced durability.

Innovation Solution

A composite coating film with a Co-based alloy powder and Cr carbide is applied using a plasma powder overlaying process, optimizing the content of C, Si, Cr, and Co to enhance peelability, oxidation resistance, and wear resistance, while controlling the microstructure to prevent cracking and maintain strength.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a coating film is formed on the surface of base metal to prevent sticking, then sticking resistance is improved, but build-up resistance deteriorates due to local adhesion of peeled-off material and oxide

Engineering Contradiction:
Improvesticking resistanceVSAvoidbuild-up formation
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention uses a composite coating film containing Cr carbide particles (20-70 vol%) dispersed in a metal matrix. The Cr carbide provides hard particles that prevent build-up adhesion, while the metal matrix ensures coating integrity and sticking resistance. This composite structure resolves the contradiction by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The coating film creates a localized hard surface layer with Cr carbide particles on the roller surface, while the base metal retains its original properties. This localized modification provides build-up resistance at the contact surface without affecting the overall roller structure, resolving the contradiction between sticking resistance and build-up prevention.

Inventive Principle:
Principle #3Local quality

2Strength

If a hard coating film is formed to improve wear resistance, then wear resistance is improved, but cracking occurs during cooling after plasma powder overlay

Engineering Contradiction:
Improvewear resistanceVSAvoidcracking during cooling
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The invention controls the carbon content in the alloy powder within a specific range (0.03-0.6 mass%) to optimize the microstructure of the coating film. By adjusting compositional parameters, the coating achieves sufficient hardness for wear resistance while maintaining microstructural stability during cooling, preventing crack formation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The coating film creates a localized hard surface layer with Cr carbide particles on the roller surface, while the base metal retains its original properties. This localized modification provides build-up resistance at the contact surface without affecting the overall roller structure, resolving the contradiction between sticking resistance and build-up prevention.

Inventive Principle:
Principle #3Local quality

3Reliability

If overlay welding is performed to form a heat resistant coating film, then oxidation resistance is improved, but the coating film becomes brittle and cracks during thermal cycling

Engineering Contradiction:
Improveoxidation resistanceVSAvoidcracking during thermal cycling
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The invention optimizes the compositional parameters of the alloy powder, specifically controlling C content (0.03-0.6 mass%), Si content (0.2-3 mass%), Cr content (22-35 mass%), and Co content (>50 mass%). These parameter adjustments create a coating film with balanced oxidation resistance and thermal shock resistance, preventing crack formation during thermal cycling.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The coating film is formed as a composite material with Cr carbide particles dispersed in a Co-based metal matrix. This composite structure provides both oxidation resistance from the Cr-containing matrix and thermal shock resistance from the controlled microstructure, resolving the contradiction between oxidation resistance and thermal cycling stability.

Inventive Principle:
Principle #40Composite materials

4Reliability

If Cr or Ni alloy is selected as base metal to improve sticking resistance, then sticking resistance is improved, but build-up resistance remains insufficient

Engineering Contradiction:
Improvesticking resistanceVSAvoidbuild-up resistance
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention applies a composite coating film containing Cr carbide particles (20-70 vol%) on the base metal surface. The Cr carbide provides hard particles that prevent build-up adhesion, while the metal matrix ensures coating integrity and sticking resistance. This composite structure resolves the contradiction by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The coating film is formed as a distinct layer segmented from the base metal, with Cr carbide particles distributed throughout the metal matrix. This segmentation allows the coating to provide specialized build-up resistance functions while the base metal provides structural support and sticking resistance, resolving the contradiction between the two requirements.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively prevents build-ups and indentation defects, ensuring long-term durability and improved quality of hot working products, with enhanced wear and oxidation resistance, thus extending the life of transfer rollers and reducing production costs.

Implementation Method 1

a composite coating film of Co-based alloy-Cr carbide which is formed by a plasma powder overlaying process

Methodology Applied
Scientific EffectPlasma powder overlaying: Plasma Spray

Implementation Method 2

enhanced wear and oxidation resistance

Methodology Applied
Scientific EffectWear resistance: Wear

Implementation Method 3

sticking may occur between the high-temperature material and the transferring member

Methodology Applied
Scientific EffectFriction: Friction

Implementation Method 4

enhanced wear and oxidation resistance

Methodology Applied
Scientific EffectOxidation resistance: Oxidation

Data Source

PatentEP2514854B1Member for conveying high-temperature materials
Publication Date: 2018.09.19 NIPPON STEEL & SUMITOMO METAL CORP
  • EP2514854B1 patent drawingFigure 1

AI summary

A high-temperature material transferring member including a coating film formed on a surface of base metal, wherein the coating film is a composite coating film using a mixed powder made up of: a Co-based alloy powder containing, in mass%, 0.03 to 0.6% of C, 0.2 to 3% of Si, 22 to 35% of Cr, and more than 50% of Co; and a Cr carbide powder, the composite coating film is formed by the plasma powder overlaying process. The high-temperature material transferring member has excellent build-up resistance particularly in a gas atmosphere of 1100°C or more. The high-temperature material transferring member has excellent in build-up resistance, oxidation resistance, and heat cracking resistance.