CO2 Drying Error Correction Apparatus

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Solution Overview

Problem

Conventional CO2 drying experiments inaccurately measure salt crystal mass due to evaporation of saline water, leading to significant errors in carbon dioxide sequestration process evaluations.

Innovation Solution

An apparatus comprising a heating jacket, transparent visual container, weighing device, vacuum pump, and control apparatus, which allows for precise measurement of evaporated water and retained salt crystals, correcting the error in salt crystal mass calculation by distinguishing between water and salt in the drying process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If the wet rock core is directly dried to measure salt crystal mass, then the measurement process is simple, but the measured mass includes both salt crystals and evaporated saline water, leading to significant error

Engineering Contradiction:
Improvesimplicity of measurement processVSAvoidaccuracy of salt crystal mass
Core Design Contradiction:
Ease of manufactureVSMeasurement precision

Solution Approach 1:

The invention segments the measurement process into two separate measurements: first measuring the mass of the wet rock core, then after drying, measuring the mass of dried rock core and separately measuring the mass of dried saline solution. This segmentation allows distinguishing between salt crystal mass and evaporated water mass, resolving the contradiction between simple process and accurate measurement.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention uses an intermediary substance (alcohol) to wash and extract the salt crystals from the dried rock core. The alcohol dissolves the salt crystals and carries them away, allowing separate measurement of salt crystal mass independent of the rock core mass. This intermediary approach enables precise measurement while maintaining operational simplicity.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If the mass difference between wet and dry rock core is used as salt crystal mass, then the calculation is straightforward, but the result is too large due to inclusion of evaporated saline water mass

Engineering Contradiction:
Improvestraightforward calculationVSAvoidaccuracy of drying effect results
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The invention segments the total mass loss into two components: mass loss from rock core drying and mass loss from saline solution evaporation. By separately measuring and calculating these components, the invention enables straightforward calculation while achieving accurate salt crystal mass determination, resolving the contradiction between ease of operation and measurement precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention uses feedback by measuring the mass of saline solution before and after evaporation, and using this information to correct the salt crystal mass calculation. The measured data feeds back into the calculation process to eliminate the error caused by including evaporated water mass, achieving both straightforward operation and accurate results.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus provides accurate results by separating the mass of evaporated water from the mass of salt crystals, thereby improving the precision of CO2 drying effect experiments and reducing errors in carbon dioxide sequestration assessments.

Implementation Method 1

the liquid evaporated to dryness is saline water, wherein salt crystals are retained in the rock core

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

an exhaust pipeline and a vacuum pipeline respectively communicated with the inside and the outside of the transparent cover are arranged on the damping table, and the vacuum pipeline can be connected to an external negative pressure source

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 3

the heating apparatus is arranged on the damping table outside the transparent cover, and the heating jacket is connected to the heating apparatus

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS12105005B1Apparatus for evaluating dried crystal error in CO<sub>2 </sub>drying experiment and use method thereof
Publication Date: 2024.10.01 SOUTHWEST PETROLEUM UNIV
  • US12105005B1 patent drawing
  • US12105005B1 patent drawing

AI summary

An apparatus for evaluating a dried crystal error in a CO2 drying experiment comprises a heating jacket, a visual container, a weighing device, a transparent cover, a control apparatus, a vacuum pump, a damping table and a heating apparatus, and can accurately dry and weigh a rock sample subjected to a carbon dioxide drying effect experiment in the visual container, so that the crystal error caused by evaporation of a solution in the rock sample in the process is calculated. This apparatus provided by the present invention has high precision and simple operation, can well evaluate the crystal error caused by the saline solution retaining in the rock sample when the rock sample is directly dried in the carbon dioxide drying effect experiment, and can correct the results of the carbon dioxide drying effect experiment compared with the prior art, thereby obtaining accurate experiment results.