CO2 Separation Heat Exchanger Segmentation to Reduce Exergy Loss

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Solution Overview

Problem

Current methods for separating carbon dioxide-rich gases at subambient temperatures suffer from significant exergy losses due to inefficient heat exchange, leading to energy inefficiencies and mechanical stresses in cryogenic applications, particularly in the cold box of CO2 capture units.

Innovation Solution

The integration of a sub-cooler in the cold box to optimize heat exchange by transferring cold from low-temperature fluids to CO2 vaporized at low pressure, allowing for indirect heat exchange between two fluids in a tube-shell exchanger, and utilizing this sub-cooled CO2 to liquefy CO2 efficiently, reducing gas production and energy consumption.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If a multi-pass exchanger is used to condense CO2 using hot fluids, then CO2 condensation is achieved, but exergy losses increase and mechanical stresses occur due to significant temperature differences

Engineering Contradiction:
ImproveCO2 condensation temperatureVSAvoidexergy loss
Core Design Contradiction:
TemperatureVSLoss of energy

Solution Approach 1:

The heat exchange process is divided into two separate exchangers: a first exchanger for initial cooling and a second exchanger for final condensation. This segmentation allows each exchanger to operate with optimized temperature differences, reducing exergy losses while achieving CO2 condensation near the triple point

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first exchanger acts as an intermediary device that pre-cools the CO2 before it enters the second exchanger. This intermediate cooling step enables the second exchanger to operate with smaller temperature differences, thereby reducing mechanical stresses and exergy losses during the critical condensation phase

Inventive Principle:
Principle #24Intermediary (Mediator)

2Temperature

If liquid CO2 is expanded to reach low temperatures, then cold is generated, but gas production increases which reduces cooling efficiency

Engineering Contradiction:
Improvecold temperatureVSAvoidcooling efficiency
Core Design Contradiction:
TemperatureVSProductivity

Solution Approach 1:

The liquid CO2 is subcooled in the first exchanger before expansion. This preliminary action of subcooling reduces the temperature of the liquid CO2 prior to expansion, which minimizes gas production during expansion and maximizes the cooling efficiency of the expanded fluid

Inventive Principle:
Principle #10Preliminary action

3Temperature

If CO2 is condensed against hot fluids with large temperature differences, then CO2 condensation is achieved, but mechanical stresses increase on heat exchanger components

Engineering Contradiction:
ImproveCO2 condensation temperatureVSAvoidmechanical stress
Core Design Contradiction:
TemperatureVSStress or pressure

Solution Approach 1:

The condensation process is segmented into two exchangers, allowing the second exchanger to operate with optimized temperature differences close to the CO2 triple point. This segmentation reduces the thermal stress on brazing and heat exchanger components while achieving effective condensation

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach minimizes exergy losses, optimizes energy consumption, and reduces mechanical stresses by effectively utilizing low-temperature cold in the cold box, enabling operation closer to the triple point of CO2, thereby enhancing the efficiency of the CO2 separation process.

Implementation Method 1

indirect heat exchange between two fluids in a tube-shell exchanger

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 2

condense the CO2 efficiently

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

the production of the cold of the unit is done by the vaporization of a liquid at sufficiently low pressure

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 4

subcooling the liquid before expansion

Methodology Applied
Scientific EffectSubcooling: Supercooling

Data Source

PatentEP2938414B1Method and apparatus for separating a carbon dioxide-rich gas
Publication Date: 2020.09.02 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP2938414B1 patent drawingFigure 1
  • EP2938414B1 patent drawingFigure 2
  • EP2938414B1 patent drawingFigure 3

AI summary

In a purification method, a carbon dioxide-rich gas is cooled in a first brazed aluminium plate-fin heat exchanger (9), the cooled gas or at least one fluid derived from the cooled gas is sent to a purification step comprising a distillation step (23), the purification step produces a carbon dioxide-rich liquid (33) which is cooled, then expanded, then sent to a second heat exchanger (35) where it is heated by means of a fluid of the method (13), the exchanger carrying out an indirect heat exchange only between the carbon dioxide-rich liquid and the fluid of the method, the carbon dioxide-rich liquid at least partially vaporises in the second exchanger and the vaporised gas (37) formed heats up again in the first exchanger to form a carbon dioxide-rich gas.