CO2 Sorbent Characterization Chamber With Humidity Feedback Control

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Solution Overview

Problem

Characterizing sorbent materials for carbon dioxide capture is challenging due to variable humidities and temperatures in the lab, making reproducible comparisons and material selection difficult without standardized testing procedures.

Innovation Solution

A controlled characterization environment system with humidity, gas, and temperature control subsystems, utilizing saturated salt solutions and automated feedback loops to stabilize sorbent materials at standardized loading conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If standardized testing procedures are implemented to improve reproducibility of sorbent material characterization, then measurement precision and reliability are improved, but device complexity and ease of operation worsen due to the need for controlled environments and multiple subsystems

Engineering Contradiction:
Improvereproducibility of sorbent material characterizationVSAvoidcomplexity of controlled environment system
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The controlled environment system is divided into separate functional subsystems: humidity control subsystem with saturated salt solution, gas control subsystem with CO2 sensor and electric valve, and temperature control subsystem with thermal conditioner and sensor. Each subsystem independently controls a specific parameter, making the overall complex system manageable through modular design and reducing interference between control functions.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The gas control subsystem implements a feedback loop where the CO2 sensor continuously monitors CO2 concentration and the microcontroller adjusts the electric valve accordingly to maintain standardized CO2 levels. Similarly, the temperature control subsystem uses feedback from the thermal sensor to adjust the thermal conditioner. These feedback mechanisms ensure precise control of environmental parameters despite external variations.

Inventive Principle:
Principle #23Feedback

2Reliability

If controlled environment subsystems are added to standardize testing conditions, then reliability of material comparison is improved, but ease of operation deteriorates due to increased system setup and maintenance requirements

Engineering Contradiction:
Improvereliability of sorbent material comparisonVSAvoidease of system operation
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The humidity control subsystem uses saturated salt solutions that automatically maintain constant humidity levels through equilibrium with the surrounding air, requiring no active control or user intervention. The system self-regulates humidity by the natural evaporation and condensation processes of the salt solutions, reducing operational complexity while ensuring reliable humidity control for sorbent material testing.

Inventive Principle:
Principle #25Self-service

3Manufacturing precision

If multiple control subsystems are integrated to maintain standardized loading conditions, then manufacturing precision of testing protocol is improved, but device complexity increases due to integration of humidity, gas, and temperature control

Engineering Contradiction:
Improveprecision of testing protocol executionVSAvoidintegration complexity of control subsystems
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The microcontroller serves as a universal control unit that manages multiple subsystems including the electric valve for gas control, the thermal conditioner for temperature control, and coordinates with the CO2 sensor and thermal sensor. This centralized control architecture allows a single device to perform multiple control functions, reducing the need for separate control units for each subsystem and simplifying the overall system integration.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables reproducible and accurate comparisons of sorbent materials by ensuring consistent initial conditions, facilitating the development of effective carbon capture technologies within a tight energy budget.

Implementation Method 1

a vessel containing a saturated salt solution

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

a vessel containing a saturated salt solution

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

a CO2 sensor within the enclosure

Methodology Applied
Scientific EffectAbsorption Spectroscopy: Absorption Spectroscopy

Implementation Method 4

an electric valve through which the interior of the enclosure is in fluidic communication with a gas supply

Methodology Applied
Scientific EffectValve: Valve

Implementation Method 5

a thermal conditioner and a thermal sensor

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 6

a thermal conditioner and a thermal sensor

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 7

the microcontroller configured to function in a gas control-feedback loop, driving the electric valve in response to the CO2 sensor

Methodology Applied
Scientific EffectFeedback: Feedback

Data Source

PatentUS20250369942A1Controlled environment system for standardizing initial conditions in co2 sorbent characterization
Publication Date: 2025.12.04 THE ARIZONA BOARD OF REGENTS ON BEHALF OF THE UNIV OF ARIZONA
  • US20250369942A1 patent drawing
  • US20250369942A1 patent drawing
  • US20250369942A1 patent drawing

AI summary

A controlled environment system for standardizing initial conditions in CO2 sorbent characterization is disclosed. The system includes an enclosure that is sealable and a humidity control subsystem having a vessel inside the enclosure, with the vessel containing a saturated salt solution. The system also includes a gas control subsystem having a CO2 sensor within the enclosure and an electric valve through which the interior of the enclosure is in fluidic communication with a gas supply. The system includes a microcontroller communicatively coupled to the CO2 sensor and the electric valve, and configured to function in a gas control-feedback loop, driving the electric valve in response to the CO2 sensor. The saturated salt solution is chosen and the gas control-feedback loop of the gas control subsystem is configured such that a characterization loading condition is established and maintained within the interior of the enclosure while the enclosure is sealed.