Liquid CO2 Sub-Cooling Using Nitrogen Heat Exchange

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Solution Overview

Problem

Existing methods for sub-cooling liquid CO2 suffer from inefficiencies, such as pressure variations leading to flow rate disturbances, gas creation, and energy loss, making them costly and environmentally impactful.

Innovation Solution

A process utilizing heat exchange between liquid CO2 and liquid nitrogen to sub-cool CO2, leveraging existing nitrogen demand on-site to recover and reuse cold energy, with a circulator ensuring efficient fluid circulation and temperature control.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If liquid CO2 is sub-cooled using conventional mechanical cooling, then the temperature is reduced, but energy consumption increases and cost rises

Engineering Contradiction:
ImproveCO2 temperatureVSAvoidenergy consumption
Core Design Contradiction:
TemperatureVSUse of energy by moving object

Solution Approach 1:

The patent converts the waste cold energy from nitrogen vaporization (which would otherwise be lost) into a useful cooling resource for sub-cooling CO2. The nitrogen evaporation process, typically a loss, is harnessed to pre-cool CO2 before it enters the mechanical cooling system, reducing the energy burden on compressors and refrigeration units.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent merges two separate processes - nitrogen vaporization and CO2 sub-cooling - into a integrated heat exchange system. The cold stream from nitrogen evaporation is combined with the CO2 cooling process through heat exchangers, creating a coupled system that achieves mutual benefit and reduces overall energy consumption.

Inventive Principle:
Principle #5Merging (Combining)

2Productivity

If liquid CO2 is sub-cooled to increase dry ice production yield, then productivity improves, but additional energy consumption is required

Engineering Contradiction:
Improvedry ice production yieldVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent applies preliminary cooling action to CO2 before it enters the mechanical refrigeration system. By using waste nitrogen cold energy to pre-sub-cool CO2, the subsequent mechanical cooling requires less energy to achieve the same final temperature, thereby increasing dry ice production efficiency without proportional energy increases.

Inventive Principle:
Principle #10Preliminary action

3Temperature

If pressure of liquid CO2 is reduced to sub-cool it, then temperature decreases, but flow rate becomes unstable due to pressure variations

Engineering Contradiction:
ImproveCO2 temperatureVSAvoidflow rate stability
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent introduces heat exchangers as intermediary devices that enable temperature reduction through heat transfer rather than direct pressure reduction. This intermediary approach allows CO2 to be sub-cooled while maintaining stable pressure and flow conditions, avoiding the flow instability that would result from direct pressure reduction.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Temperature

If mechanical cooling is used to sub-cool CO2, then temperature is reduced, but system complexity and cost increase

Engineering Contradiction:
ImproveCO2 temperatureVSAvoidcooling system complexity
Core Design Contradiction:
TemperatureVSDevice complexity

Solution Approach 1:

The patent makes the nitrogen storage system multi-functional by having it serve both its original purpose (providing gaseous nitrogen) and an additional function (providing cold energy for CO2 sub-cooling). This eliminates the need for dedicated sub-cooling equipment, reducing system complexity and avoiding additional capital investment.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enhances CO2 sub-cooling efficiency, reduces carbon footprint, and increases dry ice production yield without additional energy consumption, while maintaining system integrity and reducing costs.

Implementation Method 1

heat exchange in an exchanger with liquid nitrogen taken from a nitrogen storage tank

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 2

when there is consumption of nitrogen but no consumption of CO2, first cooling of liquid CO2 taken from the CO2 storage tank is carried out by heat exchange with liquid nitrogen

Methodology Applied
Scientific EffectVaporization: Evaporation

Data Source

PatentUS20250389388A1Process for sub-cooling co2 using a fatal cryogenic liquid
Publication Date: 2025.12.25 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE

AI summary

A process for supplying sub-cooled liquid CO2 to a site comprising a user station for the liquid CO2, from a liquid CO2 storage tank, which site contains a source of liquid nitrogen that is able to supply gaseous nitrogen to a user station for the gaseous nitrogen.