Coal-Derived Hydrocarbon Particle Purification via Density Separation

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Solution Overview

Problem

Current coal processing methods are inefficient in handling and utilizing coal fines, leading to significant waste generation and environmental hazards, as they are often too wet, dirty, or fine to transport, and lack effective methods to separate pure hydrocarbon particles from mineral matter, resulting in reduced energy value and increased emissions.

Innovation Solution

Developing methods and systems to separate coal-derived solid mineral matter from carbonaceous matter, producing coal-derived solid hydrocarbon particles that are substantially free of inherent mineral matter, using froth flotation and milling processes to achieve particle sizes below 20 microns, allowing for the creation of pure coal-derived hydrocarbon particles suitable for various industrial applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If conventional coal processing methods are used to handle coal fines, then processing cost increases, but energy content and value are reduced due to high mineral matter content

Engineering Contradiction:
Improveenergy contentVSAvoidprocessing cost
Core Design Contradiction:
Loss of energyVSEase of manufacture

Solution Approach 1:

The patent applies density separation to extract and remove mineral matter from coal fines, isolating the hydrocarbon particles from the denser mineral components. This extraction process reduces mineral matter content from typical levels above 30% to below 10%, thereby increasing energy content without requiring expensive conventional processing of the entire coal matrix

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the physical state and density parameters of the coal slurry through controlled water addition and density separation processes. By adjusting the density of the slurry phase, the process selectively separates mineral matter from hydrocarbon particles based on their density differences, achieving purification at lower cost than conventional methods

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If coal fines are removed and impounded as waste, then handling and transport problems are avoided, but significant waste generation and environmental hazards occur

Engineering Contradiction:
Improvehandling and transportVSAvoidwaste generation
Core Design Contradiction:
Ease of operationVSLoss of substance

Solution Approach 1:

The patent recovers valuable hydrocarbon particles from coal fines that would otherwise be discarded as waste. Through density separation, the process selectively removes mineral matter (which would be the waste portion) and recovers the hydrocarbon-rich particles for reuse as fuel or chemical feedstock, thereby eliminating waste generation while maintaining ease of handling

Inventive Principle:
Principle #34Discarding and recovering

Solution Approach 2:

The patent converts the harmful aspect of coal fines (high mineral matter content making them unsuitable for direct use) into a benefit by using the density difference between mineral matter and hydrocarbons as the separation mechanism. The very property that makes coal fines difficult to handle (compositional heterogeneity) becomes the basis for their purification and valorization

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Quantity of substance

If density separation techniques are used to remove extraneous ash, then bulk mineral matter is reduced, but inherent mineral matter remains dispersed in the carbonaceous matrix

Engineering Contradiction:
Improvemineral matter contentVSAvoidseparation completeness
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The patent applies sequential density separation steps that progressively separate mineral matter at different stages. The process segments the separation into multiple passes, each removing a portion of mineral matter, ultimately achieving complete separation of both extraneous and inherent mineral matter from the carbonaceous matrix

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent employs excessive action by applying density separation beyond what is minimally required to remove only extraneous ash. The process continues with additional separation steps that thoroughly remove inherent mineral matter as well, ensuring complete purification even though this requires more processing than the minimum needed for bulk ash removal

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The separation of coal-derived solid hydrocarbon particles from mineral matter enhances energy content, reduces emissions, and enables the use of coal fines in chemical and industrial applications, providing a cleaner burning fuel and increasing the value of coal products.

Implementation Method 1

The aqueous slurry is milled with milling media to reduce the particle size of the particles in the aqueous slurry to less than about 20 microns

Methodology Applied
Scientific EffectMilling: Abrasion

Implementation Method 2

The milled aqueous slurry is floated to separate particles of composite coal from particles of mineral matter

Methodology Applied
Scientific EffectFroth flotation: Froth Floatation

Implementation Method 3

The floated milled aqueous slurry is passed through a filter press to mechanically remove water from the floated milled aqueous slurry

Methodology Applied
Scientific EffectFiltration under pressure: Filter (physical)

Data Source

PatentEP4134412A1Process for obtaining coal-derived solid hydrocarbon particles
Publication Date: 2023.02.15 EARTH TECHNOLOGIES USA LIMITED(US)
  • EP4134412A1 patent drawingFigure 1
  • EP4134412A1 patent drawingFigure 2
  • EP4134412A1 patent drawingFigure 3

AI summary

The coal-derived solid hydrocarbon particles are discrete particles of coal-derived carbonaceous matter having a particle size less than about 10 µm that are substantially free of inherent or entrained mineral matter. The particles of have an average particle size in the range from 1 µm to 8 µm. The particles of coal-derived carbonaceous matter are milled to a size approximately the same as a size of coal-derived mineral matter inherent in the coal source to release inherent coal-derived mineral matter particles such that the particles of carbonaceous matter and the particles of mineral matter are discrete and separable solid particles. Following separation, less than 1.5 wt.% discrete coal-derived mineral matter particles are associated with the discrete particles of coal-derived carbonaceous matter. Particles of coal-derived solid hydrocarbon matter are blended with a gaseous or liquid hydrocarbon fuel to form a two-phase hydrocarbon fuel feedstock.