Coated Lithium Manganese Active Material for Interface Stability

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Solution Overview

Problem

Existing active materials in batteries suffer from performance deterioration due to manganese elution and resistance layer formation at the interface with electrolytes, which hinders lithium ion transfer and overall battery performance.

Innovation Solution

A coating portion containing elements like Ti, Zr, Ta, or Al and oxygen is applied to the surface of a core portion comprising lithium, manganese, and oxygen, with a specific thickness and coverage ratio to prevent manganese elution and resistance layer formation, ensuring smooth lithium ion transfer.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a coating portion is applied to the surface of the core portion to prevent manganese elution and resistance layer formation, then battery performance and reliability are improved, but the device complexity and manufacturing process complexity increase

Engineering Contradiction:
Improvebattery performanceVSAvoidcoating structure
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

A coating portion containing element A and oxygen is formed in advance on the surface of the core portion before battery assembly. This preliminary coating prevents manganese elution and resistance layer formation during subsequent battery operation, improving reliability without requiring complex operational controls.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The active material is structured as a composite with a core portion containing Li, Mn, and O, and a coating portion containing element A (such as Al, Ti, Zr, Ta, Nb) and oxygen. This composite structure combines the high capacity of the core material with the protective and conductive properties of the coating, resolving the contradiction between performance and complexity.

Inventive Principle:
Principle #40Composite materials

2Reliability

If the coating portion thickness is increased to improve protection against manganese elution, then reliability improves, but the specific surface area decreases and manufacturing precision requirements increase

Engineering Contradiction:
Improveprotection against manganese elutionVSAvoidcoating thickness control
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The coating thickness is precisely controlled within the range of 0.1-10 nm, and the amount of element A is optimized to achieve W/(S×T) > 0 and ≤ 15% by mass/(cm³/g). These parameter optimizations provide sufficient protection against manganese elution while maintaining high specific surface area and avoiding excessive manufacturing difficulty.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The coating portion is applied as an ultra-thin layer with non-uniform distribution optimized for local needs. The coating provides targeted protection where manganese elution is most problematic while minimizing overall thickness to preserve specific surface area and reduce manufacturing precision requirements.

Inventive Principle:
Principle #3Local quality

3Reliability

If element A is added to the coating portion to prevent resistance layer formation, then electrical conductivity is improved, but the amount of substance increases and cost may rise

Engineering Contradiction:
Improveelectrical conductivityVSAvoidamount of element A
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The concentration of element A in the coating is precisely controlled to optimize electrical conductivity. By adjusting the amount of element A and the coating thickness to achieve W/(S×T) > 0 and ≤ 15% by mass/(cm³/g), sufficient electrical conductivity is achieved with minimal amounts of expensive elements.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

Element A in the coating portion acts as an intermediary between the core portion and the electrolyte. It prevents direct harmful interactions while maintaining electrical conductivity, allowing the use of smaller amounts of element A compared to bulk modifications.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The coating effectively suppresses performance deterioration and enhances battery performance by preventing manganese elution and interface resistance, maintaining the core portion's functionality without increasing resistance.

Implementation Method 1

a coating portion arranged on a surface of the core portion, wherein the coating portion contains an element A (A is at least one selected from the group consisting of Ti, Zr, Ta, Nb, and Al) and elemental oxygen (O)

Methodology Applied
Scientific EffectSurface coating protection: Coatings

Implementation Method 2

ensuring smooth lithium ion transfer

Methodology Applied
Scientific EffectIon transport facilitation:

Implementation Method 3

forming a coating portion containing an element A (A is at least one selected from the group consisting of Ti, Zr, Ta, Nb, and Al) and elemental oxygen (O) through atomic layer deposition on the surface of the core portion

Methodology Applied
Scientific EffectAtomic layer deposition: Chemical Vapour Deposition

Data Source

PatentUS12531235B2Active material and process for producing the same
Publication Date: 2026.01.20 MITSUI MINING & SMELTING CO LTD

AI summary

An active material includes a core portion, and a coating portion arranged on a surface of the core portion. The core portion contains elemental lithium (Li), elemental manganese (Mn), and elemental oxygen (O). The coating portion contains an element A (A is at least one selected from the group consisting of Ti, Zr, Ta, Nb, and Al) and elemental oxygen (O). W/(T×S) is more than 0 and 15% by mass/(cm3/g) or less, wherein T (nm) represents an average thickness of the coating portion, S (m2/g) represents a specific surface area of the active material, and W (% by mass) represents an amount of element A contained in the coating portion.