Coated Ion Exchange Particles for Acid-Stable Lithium Extraction

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Solution Overview

Problem

Lithium extraction using inorganic ion exchange materials faces challenges with dissolution and degradation, particularly during lithium elution in acid and uptake from liquid resources, which reduces the performance and lifespan of these materials.

Innovation Solution

Coating ion exchange particles with materials like TiO2, ZrO2, or SiO2 to protect them from dissolution and degradation, allowing for the use of concentrated acid solutions while enabling lithium ion diffusion and hydrogen ion exchange, thereby maintaining ion exchange capacity and extending material lifespan.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If concentrated acid solution is used to elute lithium, then lithium extraction efficiency is improved, but ion exchange material dissolution and degradation worsen

Engineering Contradiction:
Improvelithium extraction efficiencyVSAvoidion exchange material stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

A coating layer comprising metal oxides (such as TiO2, ZrO2, SiO2) or their mixtures is applied to the surface of the ion exchange material particles. This coating acts as an intermediary barrier that prevents direct contact between the concentrated acid solution and the ion exchange material, thereby preventing dissolution and degradation while allowing lithium ions to diffuse through and be eluted efficiently.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If coating material is applied to protect ion exchange material, then material stability is improved, but lithium ion diffusion capability worsens

Engineering Contradiction:
Improveion exchange material stabilityVSAvoidlithium ion diffusion rate
Core Design Contradiction:
ReliabilityVSSpeed

Solution Approach 1:

The coating layer is designed with porous structure that allows lithium ions to diffuse through while providing protective function. The porous structure maintains ion exchange capability by enabling ion transport pathways, thus preventing the coating from acting as a complete barrier to lithium ion diffusion.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The coating layer parameters (thickness, porosity, composition) are optimized to balance protection and ion diffusion. By controlling these parameters, the coating provides sufficient protection against acid dissolution while maintaining adequate lithium ion diffusion rates for efficient extraction.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The coating effectively prevents dissolution and degradation of ion exchange materials, enabling repeated lithium extraction cycles with high efficiency and maintaining material performance, even in the presence of concentrated acids.

Implementation Method 1

the coating material prevents dissolution of the ion exchange material

Methodology Applied
Scientific EffectPhysical barrier protection: Coatings

Implementation Method 2

the coating material allows diffusion of lithium ions and hydrogen ions to and from the ion exchange material

Methodology Applied
Scientific EffectIon diffusion: Diffusion

Implementation Method 3

Inorganic ion exchange materials absorb lithium ions from a liquid resource while releasing hydrogen ions

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Data Source

PatentEP3538266B1Lithium extraction with coated ion exchange particles
Publication Date: 2024.08.21 LILAC SOLUTIONS INC
  • EP3538266B1 patent drawingFigure 1~2
  • EP3538266B1 patent drawingFigure 3
  • EP3538266B1 patent drawingFigure 4

AI summary

The present invention relates to the extraction of lithium from liquid resources such as natural and synthetic brines, leachate solutions from mineral, and recycles products using a coated ion exchange particle comprising an ion exchange material and a coating material.