Coating Composition with Liquid Binder and Powder Catalyst

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Solution Overview

Problem

Existing coating systems face challenges with premature curing inhibition by oxygen and limited durability due to the use of peroxides, which are harmful and only suitable for specific binder types, leading to tacky layers with low curing efficiency.

Innovation Solution

A coating composition featuring cross-linkable polymer binders in a liquid phase combined with a dry, sprinkleable powder phase containing a catalyst or its precursor, which undergoes polar reactions for controlled cross-linking, allowing for a long pot life and fast curing without radical polymerization inhibition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If peroxides are used to cure the paint layer, then curing can be achieved, but oxygen in the air causes premature inhibition of radical polymerisation resulting in a tacky layer with low degree of curing

Engineering Contradiction:
Improvecuring efficiencyVSAvoidoxygen inhibition
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent extracts the harmful peroxide curing mechanism from the system and replaces it with a carbodiimide-based crosslinking mechanism that is not susceptible to oxygen inhibition, thereby eliminating the tacky layer problem while maintaining curing functionality

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the chemical reaction mechanism from radical polymerisation (peroxide-based) to carbodiimide crosslinking, fundamentally altering the curing parameters to eliminate oxygen sensitivity and improve curing efficiency

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If peroxides are used for curing, then specific binder types can be cured, but peroxides are detrimental to health and the environment and cannot be sprinkled with bare hands

Engineering Contradiction:
Improvebinder compatibilityVSAvoidhealth and environmental harm
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent removes peroxides from the coating system entirely and substitutes them with carbodiimide crosslinking agents, eliminating the health and environmental hazards associated with peroxide handling while maintaining effective crosslinking functionality

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent employs a water-based coating composition that is environmentally benign and safe for handling, replacing the hazardous peroxide system with a safer alternative that does not require special protective measures during application

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Duration of action of stationary object

If radical polymerisation is used for cross-linking, then curing can occur, but the reaction can be inhibited by oxygen leading to tacky layers

Engineering Contradiction:
Improvecuring timeVSAvoidlayer durability
Core Design Contradiction:
Duration of action of stationary objectVSReliability

Solution Approach 1:

The patent fundamentally changes the crosslinking mechanism from radical polymerisation to carbodiimide chemistry, altering the reaction parameters to eliminate oxygen inhibition while maintaining appropriate curing speed and producing a durable, non-tacky coating layer

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables easy and safe application with a durable coating layer, providing a long pot life and preventing premature curing, while ensuring the coating is not affected by oxygen, resulting in a robust and effective curing process.

Implementation Method 1

cross-linkable by polar reaction and at least one catalyst... Polar reactions are non-radical reactions. No radical formation takes place. Polar reactions take place between nucleophiles and electrophiles and involve electron pair exchange.

Methodology Applied
Scientific EffectPolar reactions: Chemical Bonding

Implementation Method 2

one or more polymer binder components having functional groups capable of cross-linking... compounds capable of activating cross-linking of the binder components

Methodology Applied
Scientific EffectCross-linking: Chemical Bonding

Data Source

PatentUS8048482B2Paint comprising a liquid phase and an active powder phase
Publication Date: 2011.11.01 AKZO NOBEL COATINGS INT BV

AI summary

Coating composition comprising a liquid first phase comprising one or more polymer binder components having functional groups capable of cross-linking by electron pair exchange, and a second phase which is a powder material, such as sand, comprising one or more compounds capable of activating crosslinking of the binder components in the liquid phase after the second phase is exposed to the first phase. The activating compound in the second phase may include a Lewis acid or Lewis base. Alternatively, the liquid phase comprises a compound which is reactive with the activating compound in the powder phase to form a Lewis base or Lewis acid. Method of applying a coating composition curable by cross-linking chemistry based on electron pair exchange, wherein after application of a layer of the coating composition on a substrate, a powder material comprising one or more cross-linking activating compounds is sprinkled over the wet layer. The thickness of the freshly applied coating layer is less than the particle size of at least a part of the powder material. After sprinkling the powder material over the coating layer, a second coating layer is applied.