Ni-rich Cathode Coating for Battery Stability

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Solution Overview

Problem

Current lithium secondary batteries face limitations in high energy density, capacity, and lifetime due to the use of Ni-rich cathode active materials, which suffer from micro-cracking and side reactions with the electrolyte, and single-crystal lithium cobalt oxide is restricted in high voltage applications.

Innovation Solution

A composite cathode active material is developed, comprising a lithium transition metal oxide with a layered crystalline phase and a cobalt hydroxide coating layer, which stabilizes the structure and reduces interfacial reactivity, enhancing charge/discharge characteristics and lifetime.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If Ni-rich cathode active materials are used to increase capacity, then electrode capacity is improved, but micro-cracking occurs and lifetime characteristics deteriorate

Engineering Contradiction:
Improveelectrode capacityVSAvoidlifetime characteristics
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent uses a composite structure with a Ni-rich core (LiNi0.8Co0.1Mn0.1O2) and a LiCoO2 coating layer. The core provides high capacity while the coating layer prevents micro-cracking and side reactions, resolving the contradiction between high capacity and long lifetime by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent applies different material properties to different regions: the inner core uses Ni-rich material for high capacity, while the outer coating layer uses LiCoO2 for structural stability and protection. This local differentiation allows each region to perform its specific function optimally.

Inventive Principle:
Principle #3Local quality

2Volume of stationary object

If single-crystal lithium cobalt oxide is used to achieve high electrode density, then electrode density is improved, but structural stability at high voltage deteriorates

Engineering Contradiction:
Improveelectrode densityVSAvoidstructural stability at high voltage
Core Design Contradiction:
Volume of stationary objectVSStability of the object's composition

Solution Approach 1:

The patent creates a composite where LiCoO2 serves dual purposes: as the coating layer providing structural stability at high voltage, and as the base material ensuring high electrode density. The Ni-doping further stabilizes the layered structure, resolving the contradiction between density and high-voltage stability.

Inventive Principle:
Principle #40Composite materials

3Ease of manufacture

If co-precipitation method is used to synthesize cathode active material, then manufacturing process is simplified, but secondary particle formation occurs and electrode density is limited

Engineering Contradiction:
Improvesynthesis process simplicityVSAvoidelectrode density
Core Design Contradiction:
Ease of manufactureVSVolume of stationary object

Solution Approach 1:

The patent performs preliminary doping of Ni into the LiCoO2 structure during the co-precipitation process, before final formation. This preliminary action allows the use of simple co-precipitation manufacturing while achieving the desired high-density single-crystal structure with improved electrochemical performance.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composite cathode active material improves structural stability and charge/discharge performance, inhibits gas generation, and maintains high electrode density, enabling better energy and cycle retention at high voltages.

Implementation Method 1

a coating layer on a surface of the core, wherein the coating layer is formed by a cobalt hydroxide (Co(OH) 2 )

Methodology Applied
Scientific EffectChemical bonding: Chemical Bonding

Implementation Method 2

a charging and discharging mechanism is based on oxidation and reduction reactions of a transition metal in a transition metal oxide

Methodology Applied
Scientific EffectOxidation and reduction reactions: Redox Reactions

Data Source

PatentEP3509140B1Positive electrode active material for secondary battery, manufacturing method thereof, and secondary battery comprising same
Publication Date: 2022.06.22 UNIST (ULSAN NAT INST OF SCI & TECH)
  • EP3509140B1 patent drawingFigure 1
  • EP3509140B1 patent drawingFigure 2
  • EP3509140B1 patent drawingFigure 3

AI summary

Provided is a composite cathode active material including: a core including a lithium transition metal oxide, the lithium transition metal oxide being doped with nickel (Ni) and at least one element selected from Group 4 to Group 13 elements and having a layered crystalline phase belonging to the Space Group R-3m; and a coating layer on a surface of the core, the coating layer including a cobalt compound.