Cobalt Compound Synthesis for Feed Supplements

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Solution Overview

Problem

Existing cobalt compounds used in feed supplements for livestock are often toxic, poorly bioavailable, or insoluble, limiting their effectiveness in preventing Vitamin B12 deficiency in ruminant animals.

Innovation Solution

A method involving dissolving cobalt acetate tetrahydrate in water, adding a selected acid, sonicating the mixture to form fine crystals, and separating the cobalt compound, which enhances bioavailability without requiring high temperatures or grinding, using acids like lactic, propionic, or gluconic acids to produce cobalt lactate, propionate, or gluconate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If cobalt carbonate is used as a feed supplement, then it has been used for many years, but a significant portion is not taken up easily by microorganisms in the rumen

Engineering Contradiction:
ImprovebioavailabilityVSAvoiduptake efficiency
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent changes the chemical parameters of cobalt compounds by producing cobalt lactate, cobalt propionate, cobalt gluconate, and cobalt heptogluconate through specific chemical reactions. These parameter changes result in compounds with improved solubility and bioavailability compared to traditional cobalt carbonate, directly addressing the uptake efficiency problem.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If cobalt chloride is used, then it provides cobalt for Vitamin B12 synthesis, but it releases hydrogen chloride which deactivates enzymes and is an irritant

Engineering Contradiction:
ImproveVitamin B12 synthesis supportVSAvoidenzyme deactivation and irritation
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent converts the harmful hydrogen chloride release of cobalt chloride into beneficial forms by using alternative cobalt compounds (cobalt lactate, cobalt propionate, cobalt gluconate, cobalt heptogluconate) that provide cobalt for Vitamin B12 synthesis without releasing harmful hydrogen chloride, thus eliminating the harmful effect while maintaining the beneficial function.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Reliability

If cobalt oxide or cobalt hydroxide is used, then it provides cobalt, but it is very insoluble at physiological temperatures and not useful in feed supplements

Engineering Contradiction:
Improvecobalt provisionVSAvoidsolubility
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent changes the solubility parameter of cobalt compounds by producing soluble forms (cobalt lactate, cobalt propionate, cobalt gluconate, cobalt heptogluconate) through specific chemical reactions with organic acids. This parameter change transforms insoluble cobalt compounds into soluble forms that can be effectively utilized by microorganisms in the rumen.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If high temperatures, high magnetic fields or grinding are used to improve bioavailability, then the relative surface area increases, but the process complexity and energy consumption increase

Engineering Contradiction:
ImprovebioavailabilityVSAvoidprocess requirements
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent changes the chemical parameters of cobalt compounds through specific chemical reactions with organic acids (lactic, propionic, gluconic, heptogluconic acids) to produce soluble cobalt compounds. This chemical parameter change improves bioavailability and relative surface area without requiring high temperatures, high magnetic fields, or grinding, thus avoiding increased process complexity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces cobalt compounds with a high relative surface area and bioavailability for microorganisms in the rumen, improving their effectiveness in feed supplements without toxicity issues, and allows for the reuse of materials.

Implementation Method 1

dissolving cobalt acetate tetrahydrate in water at a selected temperature to form a mixture

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

sonicating the mixture for a selected time

Methodology Applied
Scientific EffectUltrasonic vibration: Ultrasonic Vibration

Implementation Method 3

separating crystals of the cobalt compound from the mixture

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 4

The step of separating may also include the substep of precipitating the crystals from the mixture by cooling the mixture

Methodology Applied
Scientific EffectCooling: Cooling

Data Source

PatentUS11753430B2Method of making cobalt compounds for feed supplements
Publication Date: 2023.09.12 VITALIX INC

AI summary

A method of making a cobalt compound for feed supplements includes the steps of dissolving cobalt acetate tetrahydrate in water to form a mixture, adding an acid to the mixture, sonicating the mixture for a selected time, removing acetic acid from the mixture, and separating crystals of the cobalt compound from the mixture.