Coffee Husk Extract Reducing Agent for Nanoparticle Synthesis

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Solution Overview

Problem

Current methods for synthesizing silver nanoparticles involve toxic and hazardous chemicals, are costly, and require additional purification steps, while also utilizing valuable plant materials, rather than waste materials, which are environmentally friendly and cost-effective.

Innovation Solution

A method using coffee seed husk extract as a reducing agent to synthesize noble metal nanoparticles and nanocomposites, such as silver and titanium oxide, which are environmentally friendly and do not require stabilizers, by mixing the extract with noble metal and transition metal oxide precursors, followed by calcination to produce highly porous nanomaterials suitable for various applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional chemical methods are used to synthesize silver nanoparticles, then nanoparticle production is achieved, but toxic and hazardous chemicals are required and additional purification steps are needed

Engineering Contradiction:
Improvesynthesis process simplicityVSAvoidtoxic chemicals and purification requirements
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent converts waste coffee seed husks, which are typically discarded as agricultural waste, into a valuable green reducing agent for nanoparticle synthesis. This transforms an environmental burden into a beneficial resource that eliminates the need for toxic chemicals while maintaining effective nanoparticle production

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The coffee seed husk extract inherently contains reducing agents that automatically reduce metal salts to nanoparticles without requiring additional stabilizers or purification steps. The system serves itself by using the extract's natural composition to complete the synthesis process in a single step

Inventive Principle:
Principle #25Self-service

2Ease of manufacture

If valuable plant materials are used as reducing agents, then nanoparticle synthesis is achieved, but cost increases and environmental friendliness decreases

Engineering Contradiction:
Improvenanoparticle synthesis capabilityVSAvoidcost and environmental impact
Core Design Contradiction:
Ease of manufactureVSQuantity of substance

Solution Approach 1:

The patent recovers value from discarded coffee seed husks by extracting reducing agents that can synthesize nanoparticles. Instead of discarding the husks after coffee bean processing, the extract is utilized for nanoparticle production, creating a cost-effective and environmentally friendly process

Inventive Principle:
Principle #34Discarding and recovering

3Stability of the object's composition

If stabilizers are added to prevent nanoparticle agglomeration, then nanoparticle stability is improved, but process complexity and cost increase

Engineering Contradiction:
Improvenanoparticle stabilityVSAvoidprocess complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The coffee seed husk extract contains natural reducing agents and stabilizing compounds that work together to produce stable nanoparticles without requiring additional stabilizers. The extract self-regulates the synthesis process, preventing agglomeration through its inherent chemical composition

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces highly crystalline, porous nanomaterials with efficient antifungal activity, reducing the need for toxic chemicals and valuable plant materials, and is scalable for bulk production, demonstrating effective biocidal properties against fungal pathogens.

Implementation Method 1

A method using coffee seed husk extract as a reducing agent to synthesize noble metal nanoparticles

Methodology Applied
Scientific EffectReduction: Reduction

Implementation Method 2

heating the mixture at a temperature in the range of 70-100° C. for a time in the range of 10-60 min

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 3

followed by calcination to produce highly porous nanomaterials

Methodology Applied
Scientific EffectCalcination: Heat Treatment

Data Source

PatentUS11661349B2Method for making coffee husk reducing agent
Publication Date: 2023.05.30 IMAM ABDULRAHMAN BIN FAISAL UNIV
  • US11661349B2 patent drawing
  • US11661349B2 patent drawing
  • US11661349B2 patent drawing

AI summary

An efficient green method for the synthesis of noble metal/transition metal oxide nanocomposite comprising reducing noble metal salt and a templating metal oxide is disclosed. The method is a one-step method comprises mixing coffee seed husk extract, a noble metal precursor, and a transition metal precursor; and filtering and drying the nanocomposite. The nanocomposite prepared by the method of the invention displays all the characteristics and biocidal activity of a composite prepared by traditional methods.