Cold Gas Filtration for Sterile Pharmaceutical Spray Drying

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Solution Overview

Problem

Current spray drying systems in the pharmaceutical industry face challenges in providing sterile air for aseptic production due to inadequate filtration of viruses and bacteria at typical operating temperatures, difficulty in sterilizing equipment without compromising gasket integrity, high costs of filters, and inefficient sterilization processes that prolong production downtime.

Innovation Solution

Implementing a 'cold gas filtration' system where the process gas is first filtered to remove all viruses and bacteria before heating, using a ULPA filter with PTFE double-layer membranes, and supplementing with blanket heaters for uniform and efficient sterilization, reducing the need for excessive insulation and minimizing particle release from heating elements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If a traditional HEPA filter is used for hot gas filtration, then the filter can operate at high temperatures, but it does not filter out all viruses and bacteria and requires excessive insulation

Engineering Contradiction:
Improveoperating temperatureVSAvoidsterilization effectiveness
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent applies cold gas filtration before heating, performing the critical filtration action at lower temperatures where ULPA filters can achieve 100% virus and bacteria retention. This preliminary filtration eliminates microorganisms before the gas enters the heating zone, making subsequent hot gas sterilization unnecessary and allowing removal of excessive insulation.

Inventive Principle:
Principle #10Preliminary action

2Ease of manufacture

If an electric process gas heater is used, then the heater is inexpensive, but it releases metal scale flakes into the process gas

Engineering Contradiction:
Improveheater costVSAvoidmetal scale contamination
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The patent extracts the heating function from the gas filtration path by using a separate heating zone. The ULPA filter removes all particles including metal scale before the heated gas enters the drying chamber, effectively taking out the contamination problem while maintaining the use of inexpensive electric heaters in a isolated heating section.

Inventive Principle:
Principle #2Taking out (Extraction)

3Reliability

If hot gas filtration is used to sterilize the system, then sterilization is achieved, but the sterilization cycle time is prolonged and production downtime increases

Engineering Contradiction:
ImprovesterilizationVSAvoidsterilization cycle time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent changes the temperature parameter during filtration by performing cold gas filtration at lower temperatures where ULPA filters achieve complete virus and bacteria removal. This eliminates the need for prolonged hot gas sterilization cycles, reducing sterilization time from hours to minutes while maintaining 100% sterilization effectiveness.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If excessive insulation is applied to maintain sterilization temperatures, then sterilization is maintained, but the system complexity and cost increase

Engineering Contradiction:
Improvesterile conditionsVSAvoidinsulation requirements
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent performs preliminary virus and bacteria removal through cold gas filtration with ULPA filters before heating. Since microorganisms are already eliminated at the filtration stage, excessive insulation and hot gas sterilization become unnecessary, allowing reduction of insulation complexity and cost while maintaining sterile conditions throughout the system.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Ensures sterile gas supply, reduces sterilization cycle time, increases production efficiency, and simplifies validation of sterilization processes, while maintaining equipment integrity and compliance with regulatory standards.

Implementation Method 1

a gas filtering system comprising a filter element comprising a porous substrate with pores having a maximum diameter of less than 1 µm

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 2

the process gas is first filtered and then the process gas is heated in a heating device which does not release particles

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 3

supplementing with blanket heaters for uniform and efficient sterilization

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentEP2158029B1Process gas filter and process for cleaning the same
Publication Date: 2019.05.29 GEA PROCESS ENG
  • EP2158029B1 patent drawingFigure 1
  • EP2158029B1 patent drawingFigure 2

AI summary

The present invention relates to a spray drying system provided with a gas filtering system, which system is intended for use in the pharmaceutical industry for aseptic production of sterile pharmaceutical products or in other industries e.g. production of food, where an intake of sterile air for the drying process is necessary. The spray drying system for providing a particulate material comprises a spray drying chamber (3), after treatment equipment (4, 5) placed downstream of the spray drying chamber and a process gas heater (2) placed upstream in relation to the spray drying chamber (3), wherein an inlet filter (1) capable of removing microorganisms at a temperature below 140 °C, is placed upstream of the process gas heater (2) and that the process gas heater (2) is a non-flaking heater.