Colloid Mill Biomass Pretreatment for Biofuel Yield

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Solution Overview

Problem

Current biomass-to-biofuel production processes face inefficiencies in converting starch-based and cellulose-based biomass into biofuels due to limitations in pretreatment methods, particularly in achieving uniform particle sizes and maximizing biofuel yields.

Innovation Solution

The use of a colloid mill or high shear milling device to reduce biomass particles to a uniform size range of 100 microns to 800 microns, combined with enzyme treatment, such as cellulase enzymes, to enhance biofuel production by increasing the availability of carbohydrates for fermentation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional pretreatment methods are used, then the process is simpler, but particle size uniformity is poor and biofuel yield is limited

Engineering Contradiction:
Improveparticle size uniformityVSAvoidpretreatment process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies segmentation by dividing the biomass into progressively smaller particle sizes through multiple grinding stages. The colloid mill breaks down large biomass particles into uniform fine particles (100-800 microns), creating a segmented size distribution that maximizes surface area for enzyme action while maintaining uniformity for consistent fermentation performance.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent changes the physical parameter of particle size from large and variable to uniformly fine (100-800 microns) using the colloid mill. This parameter change fundamentally alters the biomass characteristics, enabling better enzyme penetration and significantly improving sugar release and biofuel yield without requiring complex chemical pretreatment modifications.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If biomass is ground to very fine particles, then more carbohydrates are exposed for fermentation, but the slurry becomes unpumpable and forms matted cakes

Engineering Contradiction:
Improvecarbohydrate availabilityVSAvoidslurry pumpability
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent applies partial action by grinding the biomass to a fine but not ultra-fine size (100-800 microns). This partial size reduction exposes sufficient carbohydrates for effective fermentation while avoiding the excessive fineness that would cause slurry to become unpumpable and form matted cakes, thus maintaining operational ease.

Inventive Principle:
Principle #16Partial or excessive action

Solution Approach 2:

The patent optimizes the particle size parameter to a specific range (100-800 microns) that balances two opposing requirements: fine enough to expose carbohydrates for fermentation but coarse enough to maintain slurry flowability and pumpability. This precise parameter control resolves the contradiction between carbohydrate availability and operational ease.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If larger particles are used, then slurry remains pumpable, but fewer carbohydrates are exposed and biofuel yield decreases

Engineering Contradiction:
Improvebiofuel yieldVSAvoidparticle size for pumpability
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent uses partial size reduction to achieve the optimal balance. By grinding particles to 100-800 microns (partially reduced but not to ultra-fine sizes), sufficient carbohydrate exposure is achieved for high biofuel yield while maintaining particle size large enough to ensure slurry pumpability and prevent matted cake formation.

Inventive Principle:
Principle #16Partial or excessive action

Solution Approach 2:

The patent changes the particle size parameter from large (low yield) to an optimized range (100-800 microns) that simultaneously maximizes biofuel productivity and maintains ease of operation for pumping and processing. This parameter optimization resolves the contradiction between productivity and operational ease.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If steam treatment and supplemental CO2 are applied, then pretreatment effectiveness is enhanced, but energy consumption and process complexity increase

Engineering Contradiction:
Improvepretreatment effectivenessVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The patent extracts or removes the energy-intensive steps of steam treatment and supplemental CO2 application from the pretreatment process. By relying solely on mechanical size reduction through the colloid mill, the process achieves effective pretreatment without the additional energy consumption and complexity associated with thermal and gaseous treatments.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent applies self-service by using the mechanical energy of the colloid mill alone to achieve effective pretreatment. The biomass is pretreated effectively through size reduction without requiring external steam or CO2 inputs, making the process self-sufficient and reducing overall energy consumption while maintaining reliability.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in improved biofuel yields, increased ethanol concentration, and reduced residual starch in Distillers Dry Grains with Solubles (DDGS), making the process more efficient and economically viable by producing a higher volume of biofuels per ton of biomass.

Implementation Method 1

the colloid mill does not comprise spinning discs such as are described in US Patent Publication No. 2009/0000184... using the colloid mill to reduce and limit the overall range of the particle size of biomass

Methodology Applied
Scientific EffectShear stress: Shear Stress

Implementation Method 2

the starch is broken down (i.e. hydrolyzed) into sugars by enzymes (also known as 'liquefaction')... other enzymes, are added to break down these relatively complex sugars into simple sugars (saccharification)

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 3

Yeast is also added to the fermenter where these simple sugars are used by yeast to produce ethanol or another biofuel

Methodology Applied
Scientific EffectFermentation: Fermentation

Data Source

PatentUS8563282B2Materials and methods for converting biomass to biofuel
Publication Date: 2013.10.22 EDENIQ INC
  • US8563282B2 patent drawing
  • US8563282B2 patent drawing
  • US8563282B2 patent drawing

AI summary

This disclosure provides for materials and methods for converting biomass to biofuels. The materials include a colloid mill with or without cellulase enzymes, and the methods include the use of a colloid mill and optionally cellulose enzymes to pretreat biomass for use in a biomass to biofuel production process.