Separation Column Shielding for Uniform Liquid Distribution

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Solution Overview

Problem

In mass transfer columns, particularly air separation columns, uniform liquid distribution is critical for efficient mass transfer, but traditional designs often result in liquid droplet deflection due to the interaction between ascending vapor streams and falling droplets, leading to maldistribution and poor performance, especially at high production rates.

Innovation Solution

The introduction of a shield extending from the liquid distributor surface opposite to the riser wall creates a gap between the shield and the packing, reducing the affected droplet residence time by directing ascending vapor streams closer to the packing surface, thereby minimizing droplet deflection and enhancing uniformity of liquid distribution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If traditional liquid distributor design is used, then vapor-liquid interaction occurs in the spacing, but droplet deflection increases and liquid distribution uniformity deteriorates

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidliquid distribution uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

A shield element is introduced as an intermediary component between the liquid distributor and packing. This shield redirects the ascending vapor flow away from the falling liquid droplets, preventing harmful vapor-liquid interaction that causes droplet deflection. The shield acts as a mediator that separates the vapor and liquid phases in the spacing region, allowing vapor to flow above the shield while liquid droplets fall undeflected onto the packing, thus maintaining liquid distribution uniformity while preserving mass transfer productivity.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If spacing between liquid distributor and packing is increased, then droplet deflection may increase, but liquid distribution uniformity worsens

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidliquid distribution uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The spacing region is segmented into two distinct zones by the shield element: a lower region where liquid droplets fall freely onto the packing without vapor interference, and an upper region where vapor flows above the shield. This segmentation allows the spacing to be optimized for both purposes - sufficient height for droplet formation and fall, while the shield creates a protected zone that prevents vapor-induced deflection, thereby maintaining liquid distribution uniformity even with increased spacing for improved mass transfer.

Inventive Principle:
Principle #1Segmentation

3Productivity

If vapor flow rate is increased for higher productivity, then mass transfer efficiency improves, but droplet deflection increases and liquid distribution uniformity deteriorates

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidliquid distribution uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The shield serves as a protective intermediary that enables high vapor flow rates without compromising liquid distribution uniformity. By redirecting the vapor flow above the shield, the shield prevents vapor from interacting with falling droplets even at high vapor velocities. This allows the system to operate at high productivity levels with increased vapor flow rates while the shield maintains droplet trajectory stability, ensuring uniform liquid distribution on the packing.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design significantly reduces droplet deflection and improves mass transfer efficiency by reducing the affected droplet residence time, leading to better liquid distribution and higher performance even at high vapor flow rates.

Implementation Method 1

The introduction of a shield extending from the liquid distributor surface opposite to the riser wall creates a gap between the shield and the packing, reducing the affected droplet residence time by directing ascending vapor streams closer to the packing surface

Methodology Applied
Scientific EffectVapor flow direction control:

Implementation Method 2

The liquid falls down the mass transfer column as a result of gravity

Methodology Applied
Scientific EffectGravity: Gravitation

Implementation Method 3

Liquid streams of droplets form after passing through the liquid distribution apertures or holes of the liquid distributor and the streams of droplets fall from the liquid distributor through the spacing

Methodology Applied
Scientific EffectDroplet fall:

Data Source

PatentUS9346010B2Shielding in a separation column
Publication Date: 2016.05.24 AIR PROD & CHEM INC
  • US9346010B2 patent drawing
  • US9346010B2 patent drawing
  • US9346010B2 patent drawing

AI summary

A liquid distributor and method for distribution of a liquid in a mass transfer column, the distributor includes at least one riser comprising at least one riser wall, the at least one riser wall extends from a first surface of the distributor in a first direction of the mass transfer column; at least one shield, the at least one shield extends from a second surface of the distributor opposite the first surface and extending in a second direction opposite the first direction; and at least one liquid distribution aperture extending from the first surface of the distributor through the second surface of the distributor, the at least one shield has a length extending in the second direction such that a gap is created between the at least one shield and a packing, the height of the gap between the shield and the packing is about 10 mm to 75 mm.