Combined Light Scattering and Optical Imaging Particle Sizing

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Solution Overview

Problem

Existing methods for measuring particle size distributions face challenges in accuracy, particularly for small particles using light scattering and large particles using imaging, due to interference from background scatter and limited diffraction resolution, respectively.

Innovation Solution

Combining light scattering and optical imaging methods, where light scattering measures small particles and imaging measures large particles, with overlapping size ranges to create a comprehensive particle size distribution, using separate but synchronized light sources and sample cells to minimize interference and enhance accuracy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If light scattering is used to measure small particles, then measurement precision for small particles is improved, but background scatter interference worsens measurement accuracy for large particles

Engineering Contradiction:
Improveparticle size measurement precisionVSAvoidbackground scatter interference
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The particle size measurement range is segmented into two distinct ranges: small particles (10 nm to 1 μm) measured by light scattering and large particles (1 μm to 1 mm) measured by optical imaging. This segmentation allows each method to operate in its optimal performance range, avoiding the interference issues that arise when a single method attempts to measure the entire size range.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent transitions from a single-dimensional measurement approach (one method for all sizes) to a two-dimensional approach by combining light scattering (for small particles) and optical imaging (for large particles). This dimensional expansion in the measurement space enables comprehensive coverage of the full particle size spectrum while maintaining high precision in each segment.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Measurement precision

If optical imaging is used to measure large particles, then measurement precision for large particles is improved, but diffraction resolution limits measurement of small particles

Engineering Contradiction:
Improveparticle size measurement precisionVSAvoiddiffraction resolution limit
Core Design Contradiction:
Measurement precisionVSDifficulty of detecting and measuring

Solution Approach 1:

The measurement capability is segmented by assigning optical imaging to large particles where it excels and light scattering to small particles where it overcomes the diffraction limit. This segmentation resolves the contradiction by ensuring each method operates only in the size range where it provides superior precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent merges two complementary measurement systems—light scattering and optical imaging—into a unified particle size distribution analysis platform. By combining these methods with overlapping size ranges, the system achieves continuous coverage from 10 nm to 1 mm, eliminating the measurement gaps and resolution limits that would exist if either method were used alone.

Inventive Principle:
Principle #5Merging (Combining)

3Device complexity

If a single measurement method is used for all particle sizes, then device complexity is reduced, but measurement accuracy across the full size range deteriorates

Engineering Contradiction:
Improvemeasurement system complexityVSAvoidparticle size distribution accuracy
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The patent creates a universal particle size measurement system that can accurately measure particles across the entire size range from 10 nm to 1 mm by integrating multiple measurement functions. The system uses light scattering for small particles and optical imaging for large particles, with both methods contributing to a comprehensive particle size distribution, thus achieving multi-functionality without sacrificing accuracy.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This combination provides accurate particle size measurements across a broader range, leveraging the strengths of each method to overcome limitations in existing technologies, ensuring representative and precise particle size data.

Implementation Method 1

A first particle size distribution is determined from light scattering measurements

Methodology Applied
Scientific EffectLight scattering: Scattering

Implementation Method 2

a second particle size distribution is determined from imaging measurements

Methodology Applied
Scientific EffectOptical imaging: Photography

Data Source

PatentUS10113945B2Method and apparatus for combining measurements of particle characteristics using light scattering and optical imaging
Publication Date: 2018.10.30 RETABCH TECH
  • US10113945B2 patent drawing
  • US10113945B2 patent drawing
  • US10113945B2 patent drawing

AI summary

The present invention comprises methods and apparatus for measuring light scattering from particles and images of particles, and for combining size distributions from the measurements to produce a single size distribution over a larger size range.