Binderless Compacted Metal Powder Densification

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Solution Overview

Problem

Existing powder metallurgy methods struggle to produce materials with complex geometries and strict tolerances, often requiring binders and resulting in altered microstructures and mechanical properties.

Innovation Solution

A method involving the selection of powders with irregular random shapes and varying grain sizes, compacted and densified without binders, to achieve high relative density and maintain initial microstructure, utilizing impact compaction and controlled temperature to form microwelds between grains.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional powder metallurgy methods are used with binders, then manufacturing ease is improved, but the microstructure is altered and mechanical properties deteriorate

Engineering Contradiction:
Improveease of manufactureVSAvoidmicrostructure stability
Core Design Contradiction:
Ease of manufactureVSStability of the object's composition

Solution Approach 1:

The invention extracts and eliminates the binder component from the conventional powder metallurgy process. By using irregularly shaped metal powder particles that mechanically interlock during compaction, the patent achieves binderless consolidation, thereby preserving the original metal microstructure and properties without the need for organic or inorganic binders that would alter the material composition.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention introduces irregularly shaped metal powder particles as an intermediary mechanism to replace the binder's binding function. The irregular surfaces and interlocking geometry of the particles serve as a mechanical mediator that provides cohesion and strength without requiring chemical binders, thus maintaining microstructure stability while enabling ease of manufacture.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Manufacturing precision

If sintering is performed at high temperature, then densification is improved, but the microstructure is drastically modified and mechanical properties are altered

Engineering Contradiction:
ImprovedensificationVSAvoidmicrostructure stability
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The invention changes the compaction parameters by applying high pressure during the compaction stage to achieve sufficient densification without requiring high-temperature sintering. This parameter change allows the process to reach the necessary density threshold to eliminate porosity and achieve mechanical properties comparable to or exceeding traditional sintered parts, while avoiding microstructure modification.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the thermal field (heat-based sintering mechanism) with a mechanical field (pressure-based compaction mechanism). By substituting thermal energy with mechanical energy during consolidation, the process achieves densification through plastic deformation and particle rearrangement rather than diffusion bonding, thereby preserving the original microstructure while achieving the required density.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Strength

If binder is used to bind grains, then cohesion is improved, but the need for debinding and sintering steps increases process complexity

Engineering Contradiction:
ImprovecohesionVSAvoidprocess complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The invention extracts and removes the binder from the material system entirely. By relying on the mechanical interlocking of irregularly shaped metal particles, the process eliminates the need for binder addition, application, and subsequent removal through debinding and sintering operations, thereby simplifying the overall manufacturing process while maintaining grain cohesion.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention enables the metal powder particles to bind to each other through their own geometric characteristics (irregular shapes and interlocking surfaces) during compaction, without requiring an external binder agent. This self-binding mechanism eliminates the need for separate debinding and sintering steps, reducing process complexity while achieving the necessary cohesion for structural integrity.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces materials with high relative density and stable mechanical properties, suitable for complex geometries and micromechanics applications, without the need for binders or subsequent sintering, while maintaining the native morphology of the starting powders.

Implementation Method 1

The irregular random shape of the grains, and particularly of their external surface, including irregularly shaped hollows and peaks, allows the grains to bind by entanglement to each other during the manufacturing process

Methodology Applied
Scientific EffectPhysical entanglement:

Implementation Method 2

densifying by impact the compacted agglomerate assembly at a temperature below the melting temperature of the powder having the lowest melting temperature

Methodology Applied
Scientific EffectImpact force: Impact Force

Implementation Method 3

At the end of the densification step, the grains are permanently bound to each other by microwelds at their interfaces

Methodology Applied
Scientific EffectMicrowelding: Welding

Implementation Method 4

the assembly being brought to said temperature, prior to or during densification, for a time comprised between 3 and 30 minutes and preferably between 5 and 20 minutes

Methodology Applied
Scientific EffectControlled heating: Heating

Data Source

PatentUS11759857B2Material obtained by compaction and densification of metallic powder(s)
Publication Date: 2023.09.19 ETA SA MFG HORLOGERE SUISSE
  • US11759857B2 patent drawing
  • US11759857B2 patent drawing
  • US11759857B2 patent drawing

AI summary

The invention relates to a compacted and densified metal material having one or more phases formed of an agglomerate of grains, the cohesion of the material being provided by bridges formed between grains, said material having a relative density higher than or equal to 95% and preferably higher than or equal to 98%.