Composite Absorbent Granules for Sulfur Removal

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Solution Overview

Problem

Existing absorbents for removing sulfur compounds from hydrocarbon streams face challenges such as low absorption capacity, physical disintegration, and difficulty in maintaining integrity, especially at low temperatures and with water-saturated streams, leading to increased pressure drop and environmental concerns.

Innovation Solution

An absorbent composition in granule form, comprising iron oxides or hydroxides, a binder, water, and activated carbon, with a carbon content between 0.5% to 50% by weight, which enhances absorption capacity and mechanical strength, allowing for effective impurity removal and easier handling and recycling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If iron oxide and hydroxide absorbents are used to remove sulfur compounds, then absorption capacity is improved, but physical disintegration occurs leading to increased pressure drop

Engineering Contradiction:
Improvesulfur absorption capacityVSAvoidphysical integrity
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent applies composite materials by combining iron oxide and hydroxide with activated carbon in a specific ratio (0.5% to 50% by weight). This composite structure provides both high sulfur absorption capacity from the iron compounds and enhanced mechanical strength from the activated carbon matrix, preventing physical disintegration while maintaining absorption effectiveness.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If absorbent granules are used in water-saturated streams, then sulfur removal is effective, but granule disintegration increases

Engineering Contradiction:
Improvesulfur compound removalVSAvoidgranule stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The composite material combines iron oxide/hydroxide with activated carbon, where the activated carbon provides structural stability and resistance to water saturation effects. This composite structure maintains granule integrity in water-saturated streams while preserving the sulfur removal capability of the iron compounds.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The activated carbon component provides a porous structure that can accommodate water saturation without causing granule disintegration. The porous matrix protects the iron oxide/hydroxide particles from direct water contact that would otherwise cause disintegration, while still allowing sulfur compounds to be absorbed.

Inventive Principle:
Principle #31Porous materials

3Duration of action of stationary object

If multiple absorption equipment units are used in parallel, then continuous operation is maintained, but device complexity increases

Engineering Contradiction:
Improvecontinuous operationVSAvoidnumber of equipment units
Core Design Contradiction:
Duration of action of stationary objectVSDevice complexity

Solution Approach 1:

The patent enables single equipment unit to operate for extended periods by providing absorbent with higher durability and resistance to disintegration. The improved absorbent composition allows one unit to handle the full load for longer intervals, reducing the need for multiple parallel units while maintaining continuous operation capability.

Inventive Principle:
Principle #16Partial or excessive action

4Quantity of substance

If exhausted absorbent is removed and replaced frequently, then absorption capacity is maintained, but loss of substance increases

Engineering Contradiction:
Improveabsorption capacityVSAvoidabsorbent material loss
Core Design Contradiction:
Quantity of substanceVSLoss of substance

Solution Approach 1:

The enhanced durability and resistance to physical disintegration of the composite absorbent allow it to maintain absorption capacity for longer periods without degradation. This reduces the frequency of replacement and minimizes material loss from frequent handling and disposal of exhausted absorbent.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The absorbent composition significantly increases sulfur absorption capacity, maintains physical integrity before and after saturation, reduces material loss, and facilitates reprocessing, thereby improving operational efficiency and environmental sustainability.

Implementation Method 1

the said absorbent, and particularly activated carbon, which has the property of enhancing the capacity of the absorbent to absorb impurities contained in the streams

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

certain products formulated with metal oxides and hydroxides may be used to remove sulfur compounds from liquid or gaseous streams

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP2609985B1Use of an absorbent composition for removing contaminants, mainly sulphur compounds, contained in liquid and gaseous streams
Publication Date: 2020.09.09 CLARIANT SA

AI summary

The present invention relates to an absorbent composition composed of an iron oxide and/or hydroxide, activated carbon, promoters and binders, in the form of extruded tablets or granules, capable of absorbing impurities from fluid streams in order to eliminate the impurities, mainly sulfur compounds, contained in these streams. The present invention also relates to the methods for obtaining the absorbents, and to the use thereof for eliminating impurities contained in liquid and gaseous streams.