Concentric Ring Gas Atomizer Nozzle for ODS Steel

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Solution Overview

Problem

Existing high-pressure gas atomization nozzles struggle to produce ultra-fine oxide dispersion strengthened (ODS) ferritic stainless steel powders with a narrow particle size distribution, which is crucial for advanced power systems and additive manufacturing, due to limitations in controlling the atomizing gas structure and the resulting particle size distribution.

Innovation Solution

A gas atomizing nozzle with concentric ring arrays of discrete gas jet orifices and independent gas supply manifolds is used to control the atomizing gas structure, allowing for different pressures and compositions to enhance the production of fine atomized powders with a narrower particle size distribution, specifically targeting the production of ODS stainless steel powders with ideal size yields for additive manufacturing processes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a single ring of discrete gas jets is used, then the device complexity is reduced, but the manufacturing precision of particle size distribution deteriorates

Engineering Contradiction:
Improvenozzle structure complexityVSAvoidparticle size distribution uniformity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The gas jet system is segmented into multiple concentric rings with discrete jets in each ring, allowing independent control of gas flow patterns to achieve precise control over atomization process and particle size distribution

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The gas jet arrangement transitions from a single-plane configuration to a multi-dimensional concentric ring structure, adding radial and axial dimensions of control to achieve superior particle size uniformity

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If higher gas pressure is applied to increase atomization intensity, then the productivity of fine powder production is improved, but the manufacturing precision of particle size distribution deteriorates

Engineering Contradiction:
Improvefine powder production rateVSAvoidparticle size distribution uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The system independently controls gas pressure parameters for each concentric ring of jets, enabling optimization of pressure distribution to maintain both high productivity and narrow particle size distribution

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

Different regions of the atomization zone are provided with different gas pressure levels through the multi-ring structure, creating localized optimization zones that simultaneously achieve high production rate and uniform particle size

Inventive Principle:
Principle #3Local quality

3Manufacturing precision

If the gas jet orifice size is reduced to increase atomization fineness, then the manufacturing precision of particle size is improved, but the device complexity increases

Engineering Contradiction:
Improveultra-fine powder size controlVSAvoidnozzle orifice configuration complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The atomization function is segmented across multiple concentric rings with multiple discrete jets per ring, allowing the use of smaller individual orifices while distributing the complexity across a systematic modular structure

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Multiple rings of gas jets are nested concentrically around the melt delivery tube, creating a compact multi-layer structure that achieves fine atomization without proportionally increasing overall device complexity

Inventive Principle:
Principle #7Nested doll (Nesting)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The nozzle design achieves a more uniform and controlled production of fine atomized powders with a narrower particle size distribution, particularly in the range of 20 to 75 μm, improving the yield of ultra-fine powders and maintaining a consistent Y to O ratio, essential for advanced materials and additive manufacturing applications.

Implementation Method 1

close-coupled gas atomization: high frame rate analysis of spray-cone geometry

Methodology Applied
Scientific EffectGas recirculation flow:

Implementation Method 2

The formation of the Mach disk truncates the recirculation zone and isolates the wake region, resulting in deep aspiration at the exit orifice of the melt delivery tube

Methodology Applied
Scientific EffectMach disk formation: Shock Wave

Implementation Method 3

supersonic atomization gas along the periphery of the tube

Methodology Applied
Scientific EffectSupersonic flow:

Implementation Method 4

forced the liquid to bloom and spread or film across the transverse landing of the melt delivery tube prior to being sheared by supersonic atomization gas along the periphery of the tube

Methodology Applied
Scientific EffectShear stress: Shear Stress

Implementation Method 5

Liquid fragments or droplets are abruptly decelerated as they pass through the Mach disk and crash into the high pressure stagnation front, which helps to further disintegrate the liquid into a fine mist

Methodology Applied
Scientific EffectPressure gradient: Pressure Gradient

Implementation Method 6

Liquid fragments or droplets are abruptly decelerated as they pass through the Mach disk and crash into the high pressure stagnation front

Methodology Applied
Scientific EffectImpact force: Impact Force

Implementation Method 7

nascent atomized droplets react with small amounts of O2 within the reactive atomization gas to form an ultra-thin (t2O3)

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 8

Heat treatment of the consolidated powders results in an oxygen exchange reaction between the Cr-enriched prior particle boundary (PPB) oxide and Y-enriched IMC precipitates

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 9

Heat treatment of the consolidated powders results in an oxygen exchange reaction between the Cr-enriched prior particle boundary (PPB) oxide and Y-enriched IMC precipitates

Methodology Applied
Scientific EffectOxygen exchange reaction: Redox Reactions

Data Source

PatentUS10835959B2Atomizer for improved ultra-fine powder production
Publication Date: 2020.11.17 IOWA STATE UNIV RES FOUND INC
  • US10835959B2 patent drawing
  • US10835959B2 patent drawing
  • US10835959B2 patent drawing

AI summary

A concentric ring gas atomization nozzle with isolated gas supply manifolds is provided for manipulating the close-coupled atomization gas structure to improve the yield of atomized powders.