Condenser Spray System for Aromatic Vinyl Polymer Volatile Recovery

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Solution Overview

Problem

The existing methods for preparing aromatic vinyl compound-vinyl cyanide compound polymers face inefficiencies in condensation, leading to the discharge of uncondensed volatile components, which incur significant wastewater treatment costs and environmental pollution due to limitations in refrigerant temperature and condensation efficiency, especially with vinyl cyanide monomers of low boiling points.

Innovation Solution

The method involves using one or more condensers in series and spraying an organic solvent or aromatic vinyl monomer onto the volatile components being transferred between condensers to enhance condensation efficiency, reducing the amount of residual monomers and solvents discharged.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the temperature of the refrigerant is lowered to improve condensation efficiency, then condensation efficiency is improved, but due to installation limitations, there is a limit in lowering the temperature, resulting in discharge of uncondensed volatile components

Engineering Contradiction:
Improvecondensation efficiencyVSAvoiddischarge of uncondensed volatile components
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The condensation system is divided into multiple stages with multiple condensers connected in series. Each condenser handles a portion of the condensation process, allowing progressive cooling and condensation of volatile components at different temperature levels, thereby improving overall condensation efficiency without requiring extreme refrigerant temperatures in a single stage

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Organic solvent is sprayed onto volatile components before they enter the condenser(s). This preliminary action pre-cools the volatile components and facilitates more effective condensation in the subsequent condensation stage, reducing the discharge of uncondensed volatile components

Inventive Principle:
Principle #10Preliminary action

2Productivity

If the pressure in the condensers is increased to improve condensation efficiency, then condensation efficiency is improved, but the amount of equipment and system complexity increases

Engineering Contradiction:
Improvecondensation efficiencyVSAvoidcondensation system complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The condensation process is segmented into multiple condensers connected in series, with each condenser operating at optimized pressure and temperature conditions. This segmentation allows each unit to be simpler in design while collectively achieving high condensation efficiency

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Organic solvent acts as an intermediary substance that is sprayed onto volatile components. This intermediary facilitates heat transfer and condensation without requiring extreme pressure or temperature conditions, simplifying the overall system design while maintaining high condensation efficiency

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If two or more condensers connected in series are used to improve condensation efficiency, then condensation efficiency is improved, but the device complexity and installation space requirements increase

Engineering Contradiction:
Improvecondensation efficiencyVSAvoidcondensation system complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The condensation system is divided into multiple condensers connected in series, with each condenser handling a specific portion of the volatile components. This segmentation enables each condenser to be optimized for specific conditions, improving overall efficiency while allowing modular installation that can adapt to space constraints

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Each condenser in the series serves multiple functions: condensing volatile components, cooling the gas stream, and preparing the mixture for the next condensation stage. This multi-functionality reduces the need for additional specialized equipment, thereby limiting the increase in overall system complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces the discharge of volatile components into the atmosphere and wastewater treatment costs, improving condensation efficiency and minimizing environmental pollution by effectively condensing volatile components.

Implementation Method 1

condensation of the separated volatile components is performed using a condenser

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 2

spraying an organic solvent onto the separated volatile components being transferred from the volatilization tank to the condenser

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS11512153B2Method of preparing aromatic vinyl compound-vinyl cyanide compound polymer and apparatus for preparing the same
Publication Date: 2022.11.29 LG CHEM LTD
  • US11512153B2 patent drawing

AI summary

The present invention relates to a method of preparing an aromatic vinyl compound-vinyl cyanide compound polymer including a step of separating volatile components from a polymerization product containing an aromatic vinyl compound-vinyl cyanide compound polymer, a residual aromatic vinyl monomer, a residual vinyl cyanide monomer, and an organic solvent using a volatilization tank, and a step of condensing the separated volatile components using a condenser, wherein an organic solvent or an aromatic vinyl monomer is sprayed onto the volatile components being transferred to the condenser. Volatile components may be fully condensed in a condenser, thereby significantly reducing the amount of volatile components discharged to the outside without being condensed. Therefore, wastewater treatment costs consumed in treating the volatile components may be reduced, and the amount of vinyl cyanide monomers harmful to the human body discharged into the atmosphere may be significantly reduced.