Conditioning Gel Phase Temperature Control

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Solution Overview

Problem

Existing hair conditioning compositions fail to achieve superior conditioning benefits while maintaining a non-greasy feel the next day, as they often result in excessive solid deposition leading to lank hair.

Innovation Solution

A process involving a conditioning gel phase is developed, where the mixture of molten fatty alcohol and an aqueous isotropic solution of cationic surfactant is maintained at a controlled temperature of 55°C to 65°C, with careful temperature management and controlled addition of water and ingredients to achieve improved conditioning capabilities.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If materials are mixed in water at around 70°C using standard processes, then the conditioning composition can be manufactured, but the conditioner thickness and next-day clean feel are inferior

Engineering Contradiction:
Improveconditioning gel phase structureVSAvoidconditioner thickness and clean feel quality
Core Design Contradiction:
Manufacturing precisionVSDifficulty of detecting and measuring

Solution Approach 1:

The patent changes the temperature parameter from the conventional 70°C to a lower range of 55-65°C during the mixing of fatty alcohol and aqueous isotropic solution. This parameter change fundamentally alters the gel phase structure formation, enabling superior conditioning performance with improved thickness and next-day clean feel while using lower solids levels.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies preliminary action by carefully controlling and maintaining the temperature at 55-65°C before and during the mixing process. The fatty alcohol is pre-heated to 80-85°C to maintain it in liquid phase prior to addition, and the mixture temperature is controlled by modifying the temperature/rate of addition. This preliminary temperature control ensures the right gel phase structure forms from the outset.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If higher solids levels are used to achieve superior conditioning, then conditioning benefits improve, but the hair becomes lank and greasy the following day due to excessive deposition

Engineering Contradiction:
Improveconditioning benefitsVSAvoidexcessive solid deposition causing lank and greasy hair
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the temperature parameter to 55-65°C (lower than conventional 70°C) which fundamentally alters how the conditioning composition interacts with hair. This parameter change enables superior conditioning benefits to be achieved with lower solids levels (0.01-10% fatty alcohol), preventing excessive deposition that causes lank and greasy hair the next day.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent utilizes phase transitions by maintaining fatty alcohol in liquid phase (pre-heating to 80-85°C) before mixing, then controlling the mixture temperature to form a specific gel phase structure. The controlled phase behavior during mixing and cooling creates an optimized conditioning composition that delivers benefits without excessive solids deposition.

Inventive Principle:
Principle #36Phase transitions

3Ease of manufacture

If the temperature of the mixture is not carefully controlled, then the process is simpler, but the right conditioning gel phase structure cannot be achieved

Engineering Contradiction:
Improvemixing process simplicityVSAvoidconditioning gel phase structure
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent establishes a specific temperature parameter range of 55-65°C (most preferably 60°C) for the mixing process. This parameter specification balances manufacturing feasibility with achieving the right gel phase structure. The temperature is controlled by modifying the temperature/rate of addition of fatty alcohol to the aqueous isotropic solution, providing a practical control method.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies preliminary action by pre-heating fatty alcohol to 80-85°C to maintain it in liquid phase before addition, and by controlling the mixture temperature through modified temperature/rate of addition. This preliminary preparation simplifies the manufacturing process while ensuring the right gel phase structure forms, as the materials are already in the optimal state for mixing.

Inventive Principle:
Principle #10Preliminary action

4Object-affected harmful factors

If the weight ratio of cationic surfactant to fatty alcohol is too high, then eye irritancy increases, but if too low, then hair feels squeaky

Engineering Contradiction:
Improveeye irritancyVSAvoidsqueaky hair feel
Core Design Contradiction:
Object-affected harmful factorsVSObject-generated harmful factors

Solution Approach 1:

The patent optimizes the weight ratio parameter of cationic surfactant to fatty alcohol to specific ranges (from 1:1 to 1:10, preferably 1:1.5 to 1:8, optimally 1:2 to 1:5). This parameter optimization simultaneously reduces eye irritancy (by not using excessive cationic surfactant) and prevents squeaky hair feel (by maintaining sufficient ratio). The temperature parameter change to 55-65°C also influences this balance by affecting gel phase structure and ingredient interaction.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process results in a conditioner with superior thickness and next-day clean feel, despite lower solids levels, demonstrating enhanced conditioning performance and efficient use of ingredients.

Implementation Method 1

the fatty alcohol is maintained at a temperature sufficient to maintain the fatty alcohol in a liquid phase

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 2

The improvement thus resides in the balance of thermal energy at the point of mixing the fatty alcohol with the isotropic mixture

Methodology Applied
Scientific EffectThermal energy balance:

Data Source

PatentEP2877147B1Process for making a conditioning gel phase
Publication Date: 2018.10.31 UNILEVER IP HLDG BV

AI summary

Process for making a conditioning gel phase comprising: forming an aqueous isotropic solution of cationic surfactant; mixing the aqueous isotropic solution of cationic surfactant withmoltenfatty alcohol wherein the temperature during mixing the fatty alcohol with the isotropic cationic surfactant solution is maintained from 55oC to 65oC.