Conductive Sulphur Particle Coating for Li-S Battery Stability

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Solution Overview

Problem

State-of-the-art lithium-sulphur (Li-S) batteries face issues such as intrinsic insulating properties of sulphur and lithium sulphides limiting electron and ion transport, rapid capacity fading due to sulphur shuttling and lithium polysulphide diffusion, volume changes causing mechanical stress, and dendrite growth leading to reduced lifespan.

Innovation Solution

A method involving atmospheric pressure plasma discharge is used to apply a functional compound, such as an electrically conductive coating, onto sulphur particles, enhancing their conductivity and stability, thereby improving the performance of Li-S batteries.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If sulphur particles are used as cathode material in Li-S batteries, then high theoretical capacity and energy density are achieved, but intrinsic insulating properties limit electron and ion transport

Engineering Contradiction:
Improvetheoretical capacityVSAvoidelectron and ion transport
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies composite materials by coating sulphur particles with conductive polymers (such as polydiphenylene, polypyrrole, or polythiophene) to create a composite structure that combines the high capacity of sulphur with the electrical conductivity of the polymer coating, thereby resolving the contradiction between capacity and transport properties

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the physical and chemical parameters of the sulphur particle surface by applying functional coatings that modify surface properties, transforming the insulating sulphur surface into a conductive interface that enables efficient electron and ion transport while maintaining the high theoretical capacity

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If sulphur particles are used in Li-S batteries, then high energy density is achieved, but rapid capacity fading occurs due to sulphur shuttling and lithium polysulphide diffusion

Engineering Contradiction:
Improveenergy densityVSAvoidbattery lifespan
Core Design Contradiction:
Quantity of substanceVSDuration of action of stationary object

Solution Approach 1:

The patent applies preliminary anti-action by pre-coating sulphur particles with conductive polymer layers before battery assembly, which prevents sulphur dissolution and polysulphide diffusion from occurring in the first place, thereby eliminating capacity fading mechanisms rather than merely mitigating them

Inventive Principle:
Principle #9Preliminary anti-action

Solution Approach 2:

The conductive polymer coating acts as an intermediary layer between the sulphur particles and the electrolyte, preventing direct contact and interaction that cause sulphur shuttling and polysulphide diffusion, while still allowing efficient ion transport to maintain high energy density

Inventive Principle:
Principle #24Intermediary (Mediator)

3Quantity of substance

If sulphur particles are used in Li-S batteries, then high theoretical capacity is achieved, but volume changes during charging/discharging cause mechanical stress

Engineering Contradiction:
Improvetheoretical capacityVSAvoidmechanical stability
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent applies flexible thin film coatings of conductive polymers on sulphur particles, which can accommodate the volume expansion and contraction during charging and discharging cycles through their inherent flexibility and adhesion, thereby preventing mechanical stress and maintaining structural integrity while preserving high theoretical capacity

Inventive Principle:
Principle #30Flexible shells and thin films

4Ease of manufacture

If conventional coating methods are used on sulphur particles, then coating application is achieved, but harsh chemicals and wet chemical processes produce considerable waste streams

Engineering Contradiction:
Improvecoating applicationVSAvoidwaste streams
Core Design Contradiction:
Ease of manufactureVSLoss of substance

Solution Approach 1:

The patent replaces wet chemical coating processes with a dry plasma-based coating method, substituting chemical reactions with physical plasma deposition processes that apply functional coatings without requiring harsh chemicals or producing liquid waste streams, while maintaining effective coating application

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method results in Li-S batteries with improved energy density, reduced charging time, extended lifetime, and reduced irreversible capacity loss by controlling volume changes and dendrite growth, while being environmentally friendly and scalable.

Implementation Method 1

by means of an atmospheric pressure plasma discharge

Methodology Applied
Scientific EffectPlasma discharge: Plasma

Implementation Method 2

an atmospheric pressure plasma discharge comprising a gas and/or an activated or reactive gas flow resulting from the atmospheric pressure plasma discharge

Methodology Applied
Scientific EffectAtmospheric pressure plasma: Plasma

Data Source

PatentEP4111514B1Method for applying a functional compound on sulphur particles
Publication Date: 2025.11.19 VLAAMSE INSTELLING VOOR TECHNOLOGISCH ONDERZOEK NV (VITO)
  • EP4111514B1 patent drawingFigure 1
  • EP4111514B1 patent drawingFigure 2
  • EP4111514B1 patent drawingFigure 3~4

AI summary

The present invention is related to a method for applying a functional compound on sulphur particles by means of an atmospheric pressure plasma discharge comprising a gas or an activated gas flow resulting from the atmospheric pressure plasma discharge, wherein the coating composition comprises an inorganic electrically conductive compound, an electrically conductive carbon compound, an organic precursor compound of a conjugated polymer, a precursor of a hybrid organic-inorganic compound, or a mixture, and the functional compound provides the sulphur particles with an electrically conductive surface.