Contact Angle Measurement Sonication Droplet Removal

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Solution Overview

Problem

Existing contact angle measurement apparatuses require dismantling, cleaning, and re-filling for subsequent measurements, which is time-consuming and inefficient, especially when operating at high temperatures, and cannot remove fluid droplets from rock samples without damaging the samples.

Innovation Solution

A contact angle measurement system that uses sonication to detach fluid droplets from rock samples without removing the samples from the apparatus, allowing for repeated measurements on the same sample by transmitting sound waves through a bulk fluid, such as water, to remove the droplets while maintaining the rock sample in place.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of time

If the apparatus is dismantled and re-filled for subsequent measurements, then the fluid droplet can be removed from the rock sample, but the measurement process becomes time-consuming and inefficient

Engineering Contradiction:
Improvemeasurement timeVSAvoidoperational complexity
Core Design Contradiction:
Loss of timeVSEase of operation

Solution Approach 1:

The patent extracts the fluid droplet removal function from the mechanical dismantling process by introducing a sonicator that uses ultrasonic vibrations to detach droplets from the rock sample surface, allowing rapid removal without disassembling the apparatus

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces the mechanical system of dismantling and re-filling with an acoustic field-based sonication system that uses ultrasonic waves to remove fluid droplets, significantly reducing measurement time and operational complexity

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If the rock sample is removed from the holder for droplet removal, then the droplet can be detached, but the sample may be damaged and the measurement process is interrupted

Engineering Contradiction:
Improvesample integrityVSAvoidmeasurement efficiency
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent introduces a sonicator as an intermediary device that mediates between the need to remove droplets and the need to preserve sample integrity, using ultrasonic vibrations to detach droplets without mechanical contact or sample removal

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent replaces mechanical manipulation of the sample with acoustic field-based sonication, allowing droplet removal while the sample remains securely held, thus preventing damage and maintaining measurement continuity

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Productivity

If the apparatus is dismantled for subsequent measurements, then the droplet can be removed, but the device complexity increases and time is lost

Engineering Contradiction:
Improvemeasurement throughputVSAvoidapparatus structure
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent makes the holder assembly multi-functional by enabling it to both hold the rock sample securely and accommodate a sonicator for droplet removal, eliminating the need for dismantling and re-filling operations

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent merges the sample holding function with the droplet removal function by integrating the sonicator with the holder assembly, allowing both functions to be performed without apparatus reconfiguration

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables multiple, repeated contact angle measurements on a rock sample without dismantling the apparatus, maintaining sample integrity and reducing the time required for testing, while also allowing for precise temperature control to simulate subterranean conditions.

Implementation Method 1

The housing can transmit the sound wave to the fluid droplet on the rock sample, and the sound wave can sonically remove the fluid droplet from the rock sample

Methodology Applied
Scientific EffectSonication: Ultrasound

Data Source

PatentEP3749946B1Contact angle measurement with sonication
Publication Date: 2021.06.23 SAUDI ARABIAN OIL CO
  • EP3749946B1 patent drawingFigure 1
  • EP3749946B1 patent drawingFigure 2A
  • EP3749946B1 patent drawingFigure 2B

AI summary

A contact angle measurement system includes a housing, a rock sample holder positioned within the housing, a fluid dropper attached to the housing, and a sonicator attached to the housing. The holder can support a rock sample whose contact angle is to be measured. The fluid dropper is positioned relative to the holder to drop a fluid droplet on the rock sample when the rock sample is supported by the holder. The housing can transmit the sound wave to the fluid droplet on the rock sample, and the sound wave can sonically remove the fluid droplet from the rock sample.