Container Flow Caps With Vortex-Assisted Solvent Evaporation

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Solution Overview

Problem

Existing evaporative processes in laboratory settings are inefficient and lack effective methods to remove solvents and gases, with systems often failing to provide reliable thermal energy and vapor management, leading to issues like shearing of liquid surfaces and inadequate vapor removal.

Innovation Solution

The introduction of a gas stream at an angle close to parallel to the liquid surface, using a shallow helical guide, with a shearing effect to enhance evaporation, combined with a sealing ring for secure attachment and a system for controlled vapor exhaust, including a support rack for heating and a feedback-loop controlled heater for temperature stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a gas stream is introduced at a high velocity to accelerate evaporation, then the evaporation rate is improved, but the liquid surface is sheared and disrupted

Engineering Contradiction:
Improveevaporation rateVSAvoidliquid surface stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The patent changes the parameters of gas stream introduction by using a shallow helical guide to direct the gas at a low angle relative to the liquid surface. This geometric parameter change allows the gas to create a shearing effect on the vapor gradient without directly impacting the liquid surface, thus maintaining liquid stability while still accelerating evaporation through enhanced vapor removal.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If a helical guide is used to direct gas flow parallel to the liquid surface, then vapor removal efficiency is improved, but device complexity increases

Engineering Contradiction:
Improvevapor removal efficiencyVSAvoidstructure complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent employs a helical (curved) guide structure instead of a straight gas inlet. This curvature allows the gas flow to follow a spiral path that directs it parallel to the liquid surface, creating an effective shearing action on the vapor gradient. The helical geometry achieves superior vapor removal efficiency while remaining a relatively simple single-piece component.

Inventive Principle:
Principle #14Spheroidality (Curvature)

3Productivity

If thermal energy is increased to accelerate evaporation, then the evaporation rate is improved, but temperature control becomes more difficult

Engineering Contradiction:
Improveevaporation rateVSAvoidtemperature control
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent incorporates a feedback-loop controlled heater that monitors and adjusts thermal energy input to maintain stable temperature conditions. This feedback mechanism ensures that while sufficient heat is provided to accelerate evaporation, the temperature remains controlled and predictable, preventing runaway heating and ensuring reliable, repeatable results.

Inventive Principle:
Principle #23Feedback

4Ease of operation

If a sealing ring is added to facilitate device attachment, then ease of operation is improved, but device complexity increases

Engineering Contradiction:
Improvedevice attachmentVSAvoidcomponent count
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The patent uses a flexible sealing ring (typically made of elastomeric material) that provides effective sealing between the device and the vial or container. This thin, flexible component is easily integrated into the device structure and requires no complex assembly mechanisms, providing secure attachment and reliable sealing with minimal added complexity.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach accelerates the evaporation process by creating a vortex for efficient solvent removal, maintains temperature control, and ensures safe, contained vapor exhaust, suitable for various container sizes and shapes, while minimizing chemical degradation and footprint.

Implementation Method 1

produce a shearing effect on a vapor gradient that forms as an equilibrium phenomenon at the surface of a liquid. The shearing effect removes the vapor layer, thus driving equilibrium to produce more vapor which accelerates an evaporative process.

Methodology Applied
Scientific EffectShear stress: Shear Stress

Implementation Method 2

heating and thermal energy systems are provided

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 3

introducing a gas stream at an angle as close to parallel to a surface of the liquid as possible... provide a vortexing action in a liquid provided within a vial or container

Methodology Applied
Scientific EffectVortex: Vortex Ring

Data Source

PatentUS12434172B2Methods and systems for managing fluid flow in containers
Publication Date: 2025.10.07 THE GOVERNMENT OF THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY DEPARTMENT OF HEALTH & HUMAN SERVICES
  • US12434172B2 patent drawing
  • US12434172B2 patent drawing
  • US12434172B2 patent drawing

AI summary

Systems and methods for managing fluid flow in and evaporating solvents from containers are provided. In various embodiments, systems of the present disclosure provide for cap or cover members operable to be provided with vials or containers comprising one or more fluids. The caps are further operable to direct air and gas flow into and out of the containers. In some embodiments, supporting structures and heating elements are provided to enhance and assist various processes.