Continuous Hydrogen Pulverization Device for Rare Earth Permanent Magnetic Alloy

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Solution Overview

Problem

Conventional hydrogen pulverization devices for rare earth permanent magnetic alloys face challenges in collecting magnetic powder under inert gas protection, have low cooling speeds, long operation periods, and high power consumption, along with transmission part deformation and short life due to hotspot placement.

Innovation Solution

A continuous hydrogen pulverization method and device that involves a tall and thin feeding tank hung on a transmission device, with a process that includes hydrogen adsorption, dehydrogenation, and cooling under vacuum and inert gas protection, using isolation valves to connect rooms in series, and inert gas circulating cooling to improve efficiency and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a conventional rotary hydrogen pulverization furnace is used, then the magnetic powder can be processed, but it is difficult to collect the magnetic powder under the protection of inert gases

Engineering Contradiction:
Improvecollection efficiency of magnetic powderVSAvoiddifficulty in collecting magnetic powder under inert gas protection
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The furnace is divided into three separate rooms (hydrogen adsorption room, heating dehydrogenation room, and cooling room) connected in series, allowing each room to perform a specific function independently. This segmentation enables the magnetic powder to be processed and collected in separate stages under appropriate protective atmospheres, solving the collection difficulty.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent uses inert gas circulation in the cooling room to protect the magnetic powder during cooling and collection. The inert gas atmosphere prevents oxidation and facilitates easy collection of the magnetic powder without exposure to air, directly addressing the collection difficulty under protective atmosphere.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Speed

If a conventional rotary hydrogen pulverization furnace is used, then the processing can be completed, but the cooling speed is low

Engineering Contradiction:
Improvecooling speedVSAvoidcooling time
Core Design Contradiction:
SpeedVSDuration of action of moving object

Solution Approach 1:

The patent introduces a gas circulation cooling system using inert gas flow through the cooling room. This pneumatic cooling method significantly increases the cooling speed compared to conventional passive cooling, reducing the cooling time while maintaining protective atmosphere.

Inventive Principle:
Principle #29Pneumatics and hydraulics

3Productivity

If a conventional rotary hydrogen pulverization furnace is used, then the processing can be completed, but the operation period is long that may take dozens of or even over thirty hours

Engineering Contradiction:
Improveproduction capacityVSAvoidoperation period
Core Design Contradiction:
ProductivityVSDuration of action of moving object

Solution Approach 1:

The three rooms are connected in series and operate continuously with material flowing from one room to the next. The hydrogen adsorption room operates continuously, followed by heating and cooling stages, eliminating idle time between operations. This continuous process dramatically reduces the total operation period from dozens of hours to a much shorter duration while increasing production capacity.

Inventive Principle:
Principle #20Continuity of useful action

4Temperature

If an external-heating muffle furnace is used, then the heating can be performed, but it takes a lot of power

Engineering Contradiction:
Improveheating temperatureVSAvoidpower consumption
Core Design Contradiction:
TemperatureVSUse of energy by moving object

Solution Approach 1:

The patent extracts the heating function from a separate external muffle furnace and integrates it directly into the heating dehydrogenation room. This allows for more efficient heat transfer and reduced energy loss, lowering power consumption while maintaining the required heating temperature for dehydrogenation.

Inventive Principle:
Principle #2Taking out (Extraction)

5Ease of operation

If transmission parts are placed in a hotspot area, then the feeding mechanism can operate, but the transmission parts experience deformation and short life

Engineering Contradiction:
Improvefeeding mechanism operationVSAvoidlife of transmission parts
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent extracts the transmission mechanism from the high-temperature hotspot area and places it in a separate cooling room or ambient temperature zone. This separation protects the transmission parts from thermal deformation and extends their service life while maintaining continuous feeding operation through the connected room system.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enhances the consistency and performance of the rare earth permanent magnetic alloy powder, reduces oxygen content, increases production capacity, and extends the life of transmission parts while saving power, resulting in improved product quality and reduced maintenance needs.

Implementation Method 1

filling with hydrogen to 0.5-0.15 MPa after a vacuum pressure is lower than 50 Pa or a volume content of oxygen is less than or equal to 0.1%, keeping for 10 ∼120 min

Methodology Applied
Scientific EffectHydrogen adsorption: Adsorption

Implementation Method 2

heating when the pressure in the heating dehydrogenation room is less than 0.1 Pa, a highest heating temperature is 500 ∼900° C. with a heating time of 4 ∼20 h

Methodology Applied
Scientific EffectDehydrogenation: Desorption

Implementation Method 3

starting a fan for driving the inert gases into a vent tube of the feeding tank through a cambered deflector on an internal wall of the cooling room; after the inert gases enters the vent tube, cooling the feeding tank and the alloy slices in the cooling room with the inert gases

Methodology Applied
Scientific EffectConvection cooling: Convection

Implementation Method 4

cooling the heated inert gases by a heat exchanger before being blown to the cambered deflector for providing inert gas circulating cooling

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Data Source

PatentUS9543063B2Continuous hydrogen pulverization method and production device of rare earth permanent magnetic alloy
Publication Date: 2017.01.10 SHENYANG GENERAL MAGNETIC
  • US9543063B2 patent drawing
  • US9543063B2 patent drawing
  • US9543063B2 patent drawing

AI summary

A continuous hydrogen pulverization method of a rare earth permanent magnetic alloy includes: providing a hydrogen adsorption room, a heating dehydrogenation room and a cooling room in series, applying hydrogen adsorption, heating dehydrogenation and cooling on a rare earth permanent magnetic alloy in the production device at the same time, wherein collecting and storing under an inert protection atmosphere can also be provided. Continuous production is provided under vacuum and the inert protection atmosphere in such a manner that an oxygen content of the pulverized powder is low and a proportion of single crystal in the powder is high.