Continuous Toner Production Using Spinning Disc Reactors

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing toner production processes are inefficient, taking many hours and struggling with batch-to-batch consistency due to handling bulk materials, and lack the ability to produce toner quickly and consistently.

Innovation Solution

A continuous process using spinning disc reactors and rotating tubular reactors to aggregate and coalesce toner particles, allowing for precise control of temperature, shear rate, and residence time, resulting in consistent toner production with sizes ranging from 1 micron to 20 microns.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If batch process is used for toner production, then handling of bulk materials is simplified, but production time increases to many hours and batch-to-batch consistency deteriorates

Engineering Contradiction:
Improvehandling of bulk materialsVSAvoidproduction time
Core Design Contradiction:
Ease of operationVSProductivity

Solution Approach 1:

The patent implements continuous emulsion polymerization and continuous aggregation/coalescence processes, eliminating batch-to-batch interruptions. The continuous operation maintains consistent reaction conditions and eliminates the many-hour downtime associated with batch processing, directly reducing production time while improving productivity.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent replaces traditional mechanical mixing and bulk material handling with continuous fluid processing systems. The continuous injection of monomers, initiators, and aggregating agents into reaction vessels eliminates the need for manual bulk material handling and enables precise control of reaction parameters, improving both ease of operation and productivity.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Device complexity

If batch process is used for toner production, then equipment simplicity is maintained, but batch-to-batch consistency deteriorates due to variations

Engineering Contradiction:
Improveequipment simplicityVSAvoidbatch-to-batch consistency
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The patent incorporates feedback mechanisms that continuously monitor reaction parameters such as temperature, pH, and monomer conversion. Real-time feedback allows for dynamic adjustment of reaction conditions, ensuring consistent toner properties across continuous production runs and eliminating batch-to-batch variations without requiring complex equipment.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent maintains consistent reaction parameters (temperature, pH, monomer feed rates, initiator concentrations) throughout the continuous process. By controlling parameters within narrow ranges and maintaining steady-state conditions, the patent achieves high manufacturing precision while keeping equipment relatively simple.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If continuous process is used for toner production, then production time is reduced and consistency is improved, but process complexity increases

Engineering Contradiction:
Improveproduction timeVSAvoidprocess complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent divides the continuous process into distinct functional stages: emulsion polymerization, aggregation, and coalescence. Each stage is performed in separate but continuously operated units, allowing for optimized conditions in each step while maintaining overall process simplicity. This segmentation enables reduced production time without excessive complexity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent employs multi-functional reaction vessels that can perform multiple operations sequentially or simultaneously. For example, reaction vessels serve as both polymerization reactors and aggregation chambers, reducing the number of separate equipment pieces needed and simplifying the overall process despite continuous operation.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Device complexity

If batch process is used for toner production, then process control is simplified, but manufacturing efficiency deteriorates

Engineering Contradiction:
Improveprocess controlVSAvoidmanufacturing efficiency
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The continuous process eliminates idle time between batches and maintains productive operations without interruption. Monomers, initiators, and aggregating agents are continuously fed into reaction vessels, and toner is continuously produced and collected, maximizing manufacturing efficiency while keeping control mechanisms relatively simple through steady-state operation.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The continuous process is designed to be self-regulating, where reaction conditions automatically stabilize and maintain optimal levels without frequent manual intervention. The system serves itself by maintaining steady-state conditions through continuous operation, improving manufacturing efficiency without requiring complex control systems.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The continuous process significantly reduces production time, enhances batch-to-batch consistency, and allows for precise control of toner properties, leading to more efficient and high-quality toner production with improved energy efficiency and reduced waste.

Implementation Method 1

The technology operates by the use of high gravity fields created by rotation of a disc surface causing fluid introduced to the disc surface at its axis to flow radially outward under the influence of centrifugal acceleration

Methodology Applied
Scientific EffectCentrifugal force: Centrifugal Force

Implementation Method 2

spinning disc reactor at a temperature from about 35° C. to about 75° C. and a pH from about 3.5 to about 7 to form aggregated toner particles

Methodology Applied
Scientific EffectShear mixing: Shear Stress

Implementation Method 3

The aggregated toner particles are continuously coalesced in a second reactor which can include a rotating tubular reactor at a temperature from about 80° C. to about 100° C.

Methodology Applied
Scientific EffectThermal coalescence: Heating

Data Source

PatentUS7507517B2Toner processes
Publication Date: 2009.03.24 XEROX CORP
  • US7507517B2 patent drawing
  • US7507517B2 patent drawing
  • US7507517B2 patent drawing

AI summary

Continuous processes for producing toner compositions are provided utilizing spinning disc reactors, rotating tubular reactors, or combinations thereof.