Conversion Element Production via Acidic Silicate Precipitation

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Solution Overview

Problem

Existing conversion elements in optoelectronic components, particularly inorganic light-emitting diodes, suffer from low aging stability and lack cost-effective production methods, which affects their high temperature and light resistance.

Innovation Solution

A method involving an acidic medium with a pH of less than 2, where a conversion material is added and mixed with a silicate solution of 2 to 10,000 poise viscosity, resulting in a precipitate of conversion material and silicon dioxide, which is then washed and cured to produce a stable conversion element.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conversion elements are made of silicon or ceramic matrix material with embedded conversion material, then wavelength conversion function is achieved, but aging stability and temperature/light resistance are low

Engineering Contradiction:
Improveaging stabilityVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent changes the chemical composition parameters of the matrix material by incorporating specific metal oxides (Bi2O3, ZnO, B2O3) in controlled amounts to improve aging stability and temperature resistance while maintaining manufacturability through established ceramic processing techniques

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite matrix material combining traditional ceramic components with additional metal oxides (Bi2O3, ZnO, B2O3) to achieve enhanced aging stability and temperature/light resistance while maintaining the wavelength conversion functionality through embedded conversion material particles

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If conventional production methods are used for conversion elements, then manufacturing is achieved, but cost-effectiveness is poor

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidcost-effectiveness
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent combines multiple functions into a single manufacturing process by simultaneously forming the matrix material and embedding conversion material particles in one sintering step, eliminating separate processing steps and reducing overall manufacturing cost

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent enables the matrix material to self-encapsulate the conversion material particles during the sintering process, eliminating the need for separate encapsulation steps and reducing manufacturing complexity and cost

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces a conversion element with high temperature and light resistance, ensuring long-term stability and cost-effectiveness, suitable for optoelectronic components like LEDs that emit blue, green, red, or white light.

Implementation Method 1

Adding a silicate solution with a viscosity of 2 to 10000 poise to the mixture produced in step B) such that the pH during the addition in step C) is less than 2, obtaining a precipitate comprising the conversion material and silicon dioxide as a matrix material

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 2

Washing the precipitate with a washing medium having a pH of less than 2

Methodology Applied
Scientific EffectWashing:

Implementation Method 3

Hardening the precipitate to produce the conversion element

Methodology Applied
Scientific EffectHardening:

Data Source

PatentEP3334800B1Method for producing a conversion element
Publication Date: 2019.10.02 OSRAM OPTO SEMICON GMBH & CO OHG
  • EP3334800B1 patent drawingFigure 1A~1F
  • EP3334800B1 patent drawingFigure 2A~2C
  • EP3334800B1 patent drawingFigure 3A~3F

AI summary

The invention relates to a method for producing a conversion element (100) for an optoelectronic component (110) having the following steps: A) providing an acidic medium (1) with a pH value of less than 2, B) adding a conversion material (2) into the acidic medium (1), C) adding a silicate solution (3) with a viscosity of 2 to 10000 P to the mixture produced in step B) such that the pH value during the addition process in step C) is less than 2, wherein a precipitation (4) is obtained which comprises the conversion material (2) and silicon dioxide (41) as the matrix material, D) separating the precipitation (4), E) washing the precipitation (4) using a washing medium (6), said washing medium (6) having a pH value of less than 2, and F) curing the precipitation (4) in order to produce the conversion element (100).