Ethylene-Carboxylic Acid Copolymer Dispersion Viscosity Control

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Solution Overview

Problem

High concentrations of ethylene-carboxylic acid copolymers in aqueous dispersions lead to increased viscosity and gelation, deteriorating coating properties and making it difficult to achieve a balance between high concentration and low viscosity, which is essential for effective application as a coating, sealing, or adhesive.

Innovation Solution

Incorporating an inorganic salt compound, such as calcium chloride (CaCl2) or sodium sulfite (Na2SO3), in a specific weight percentage into the dispersion to reduce viscosity and improve dispersibility, allowing for a high concentration of ethylene-(meth)acrylic acid copolymer while preventing gelation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the concentration of ethylene-carboxylic acid copolymer in aqueous dispersion is increased, then the efficiency of coating, sealing, and bonding is improved, but the viscosity of the dispersion increases and gelation occurs, deteriorating coating properties

Engineering Contradiction:
Improveefficiency of coating, sealing, and bondingVSAvoidviscosity and gelation
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

An inorganic salt compound acts as an intermediary substance that mediates between the high copolymer concentration requirement and the viscosity/gelation constraint. The inorganic salt modifies the interaction between copolymer chains and water, enabling high concentration dispersions without gelation by changing the electrostatic or steric interactions in the system.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes physical or chemical parameters of the dispersion system by introducing an inorganic salt compound. This parameter change (addition of inorganic salt) allows the system to accommodate high copolymer concentrations while maintaining low viscosity and preventing gelation, thus resolving the contradiction between concentration and stability.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the concentration of ethylene-carboxylic acid copolymer in aqueous dispersion is increased, then transportation costs are reduced, but the viscosity increases and gelation occurs, making the dispersion unsuitable for coating applications

Engineering Contradiction:
Improveconcentration of ethylene-carboxylic acid copolymerVSAvoidcoating properties
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The inorganic salt compound serves as a mediator that enables high concentration dispersions to maintain good coating properties. It prevents the copolymer chains from aggregating and forming gels, thereby keeping the dispersion flowable and applicable despite the high copolymer content.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

By changing the chemical environment through inorganic salt addition, the system achieves high copolymer concentration while maintaining suitable viscosity and coating properties. The inorganic salt modifies the solvation structure and inter-chain interactions, allowing the dispersion to remain processable at high concentrations.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The addition of inorganic salts effectively reduces viscosity, enhancing the coating properties and preventing gelation, enabling the use of high-concentration ethylene-(meth)acrylic acid copolymer dispersions as efficient coating, sealing, or adhesive agents.

Implementation Method 1

adding an inorganic salt compound to the mixed solution; wherein the inorganic salt compound includes at least one of calcium chloride (CaCl2) and sodium sulfite (Na2SO3)

Methodology Applied
Scientific EffectElectrostatic effect: Electrostatics

Data Source

PatentEP3805296B1Aqueous dispersion of ethylene-carboxylic acid copolymer and method of preparing the same
Publication Date: 2025.01.01 SK INNOVATION CO LTD
  • EP3805296B1 patent drawingFigure 1~3
  • EP3805296B1 patent drawingFigure 4~5
  • EP3805296B1 patent drawingFigure 6

AI summary

A method of preparing an aqueous dispersion of an ethylene-carboxylic acid copolymer according to exemplary embodiments of the present invention includes: mixing 30 % by weight or more of an ethylene-(meth)acrylic acid copolymer, a basic compound, and water to form a mixed solution; and adding an inorganic salt compound to the mixed solution. Therefore, the aqueous dispersion of the ethylene-carboxylic acid copolymer may be effectively dispersed.