Copolymer Polymer Electrolyte for Room-Temperature High-Voltage Batteries

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Solution Overview

Problem

Lithium secondary batteries face challenges due to the high crystallinity of polyethylene oxide (PEO) at room temperature, leading to low ionic conductivity and instability at higher voltages, which limits their application in high-voltage lithium battery applications.

Innovation Solution

A polymer electrolyte is developed using a copolymer with alkylene oxide repeating units in both the main and side chains, reducing crystallinity and incorporating ester groups and halogen atoms for improved oxidation resistance, allowing for enhanced ionic conductivity and stability at higher voltages.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If polyethylene oxide (PEO) is used as polymer electrolyte, then ionic conductivity is improved at high temperature, but crystallinity increases at room temperature causing low ionic conductivity

Engineering Contradiction:
Improveionic conductivityVSAvoidoperating temperature requirement
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The patent uses a copolymer combining PEO units with PPO (polypropylene oxide) units to create a composite polymer structure. The PPO units interrupt the crystalline packing of PEO, reducing overall crystallinity while maintaining ionic conductivity pathways. This composite approach allows the electrolyte to function at room temperature without requiring external heating.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent modifies the chemical composition parameters of the polymer by incorporating different mole ratios of PEO and PPO units. By adjusting these compositional parameters, the patent optimizes the balance between crystallinity and ionic conductivity, enabling room-temperature operation with sufficient ionic transport properties.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If PEO is used for high-voltage lithium battery applications, then capacity is improved, but oxidation stability deteriorates at voltages above 3.8 V

Engineering Contradiction:
Improvebattery capacityVSAvoidoxidation stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The copolymer structure combines PEO segments (which provide ionic conductivity and lithium solvation) with PPO segments (which offer oxidation resistance). This composite material approach allows the electrolyte to withstand higher voltages without oxidation while maintaining adequate ionic transport for high-capacity battery operation.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent creates local regions with different chemical properties within the polymer chain. The PPO units provide localized oxidation resistance at the polymer-electrode interface, while the PEO units maintain ionic conductivity in the bulk. This spatial differentiation of functional properties allows simultaneous achievement of high voltage stability and high capacity.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The polymer electrolyte exhibits improved ionic conductivity and high-voltage stability, enabling its use in lithium batteries without the need for additional heating, thus enhancing the performance and reliability of lithium secondary batteries.

Implementation Method 1

PEO has a low ionic conductivity due to high crystallinity at room temperature... The copolymer includes a first repeating unit and a second repeating unit... reducing crystallinity

Methodology Applied
Scientific EffectCrystallinity reduction through copolymer structure: Crystallisation

Implementation Method 2

incorporating ester groups and halogen atoms for improved oxidation resistance... PEO is oxidized at a high voltage of about 3.8 V (vs. Li), but the copolymer maintains stability at higher voltages

Methodology Applied
Scientific EffectOxidation resistance through chemical composition: Oxidation

Implementation Method 3

The polymer electrolyte exhibits improved ionic conductivity... The copolymer includes alkylene oxide repeating units in both the main and side chains, reducing crystallinity and incorporating ester groups and halogen atoms for improved oxidation resistance

Methodology Applied
Scientific EffectIonic conduction through polymer matrix: Conduction (electrical)

Data Source

PatentEP3509149B1Polymer electrolyte, polymer, electrochemical device, and method of preparing the polymer
Publication Date: 2023.09.13 SAMSUNG ELECTRONICS CO LTD
  • EP3509149B1 patent drawingFigure 1
  • EP3509149B1 patent drawingFigure 2
  • EP3509149B1 patent drawingFigure 3

AI summary

A polymer electrolyte including a copolymer represented by Formula 1; and a lithium salt: wherein, in Formula 1, R1, R2, R3, R4, R5, R6, R7, R8, R9, R10, R11, R12, R13, R14, R15, R16, R17, L1, n1, x, y, and z are as disclosed herein.