Copolymer-Stabilized Hydrogen Peroxide for Tooth Bleaching

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Solution Overview

Problem

Current tooth bleaching agents, such as hydrogen peroxide, are unstable in aqueous formulations and do not effectively release the bleaching agent specifically at the tooth surface, leading to inefficient whitening.

Innovation Solution

A copolymer comprising repeat units from N-vinylpyrrolidone and comonomers like vinylphosphonic acid is used to stabilize hydrogen peroxide, enhancing its affinity for tooth surfaces and controlled release at the desired site, thereby improving tooth bleaching efficacy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If hydrogen peroxide is used as a bleaching agent in aqueous formulations, then tooth bleaching can be achieved, but the hydrogen peroxide becomes unstable and breaks down prematurely during storage

Engineering Contradiction:
Improvestability of hydrogen peroxideVSAvoidbleaching efficacy
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent uses a copolymer as an intermediary substance to stabilize hydrogen peroxide in aqueous formulations. The copolymer forms a complex with H2O2, preventing premature decomposition while allowing controlled release at the tooth surface. This mediator enables the coexistence of stability and efficacy in the same formulation.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention creates a composite system by combining hydrogen peroxide with a specifically designed copolymer. This composite material (polymer-H2O2 complex) exhibits both the stability needed for storage and the bleaching activity needed for efficacy, resolving the contradiction between these two properties.

Inventive Principle:
Principle #40Composite materials

2Reliability

If conventional polymers are used to stabilize hydrogen peroxide, then stability is improved, but the bleaching agent is not released specifically at the tooth surface

Engineering Contradiction:
Improvestability of hydrogen peroxideVSAvoidtargeted release at tooth surface
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The copolymer is designed with specific local properties: hydrophilic segments that interact with saliva and tooth surfaces, and hydrophobic segments that stabilize the peroxide. This local differentiation enables the complex to remain stable during storage but release H2O2 specifically at the tooth surface where saliva contact occurs.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent changes the chemical parameters of the stabilizing polymer by using a copolymer with specific functional groups (carboxylic acid, sulfonic acid, or phosphate groups) instead of conventional polymers. These parameter changes enable both stability and targeted release at the tooth surface through electrostatic interactions and saliva-triggered dissolution.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If anhydrous formulations are used to prevent hydrogen peroxide breakdown, then stability is improved, but the formulation complexity and manufacturing difficulty increase

Engineering Contradiction:
Improvestability of hydrogen peroxideVSAvoidformulation simplicity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The invention changes the formulation parameter from anhydrous to aqueous by introducing a polymer-H2O2 complexing agent. This parameter change allows water to be present in the formulation without causing premature peroxide decomposition, as the polymer protects the H2O2 from breakdown even in the presence of water, simplifying manufacturing.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The copolymer-stabilized hydrogen peroxide composition effectively releases hydrogen peroxide at the tooth surface, enhancing tooth whitening and maintaining stability, even in anhydrous toothpaste formulations.

Implementation Method 1

compositions comprising a peroxidic compound and this particular copolymer for tooth bleaching

Methodology Applied
Scientific EffectComplex formation:

Implementation Method 2

enhancing its affinity for tooth surfaces and controlled release at the desired site

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

hydrogen peroxide (also referred to hereinafter as H2O2 or H2O2) can be used as a bleaching agent in order to whiten the enamel

Methodology Applied
Scientific EffectDecomposition: Decomposition (biological)

Data Source

PatentUS10154953B2Use of a composition for bleaching teeth
Publication Date: 2018.12.18 BASF SE

AI summary

The present invention relates to the use of a composition comprising a peroxidic compound and a particular, generically defined copolymer for tooth bleaching.