Copper Lithium Heptaborate Phosphor for 3D Dosimetry

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Solution Overview

Problem

Existing thermoluminescent dosimeters face challenges in accurately measuring three-dimensional dose distribution due to overlapping emission intensity distributions, low emission intensity, and absorption of thermoluminescence by binders, requiring complex corrections and inadequate heat resistance.

Innovation Solution

A thermoluminescent phosphor comprising copper-containing lithium heptaborate with a monomodal emission intensity distribution in a visible range, resistant to heat, and suitable for use with epoxy resin binders, eliminating the need for near-infrared cut filters and simplifying dose calculations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If manganese-containing lithium tetraborate is used as thermoluminescent material, then tissue equivalence is achieved, but emission intensity distribution overlaps with heating-caused emission requiring complex corrections

Engineering Contradiction:
Improvedose measurement accuracyVSAvoidcorrection complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent changes the chemical composition parameters by using copper-containing lithium heptaborate instead of manganese-containing lithium tetraborate, and adjusts the emission wavelength range to 400-600 nm to separate from heating-caused emission, thereby eliminating the need for complex corrections while maintaining tissue equivalence

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the potential harm of heating-caused emission overlap into a benefit by carefully selecting the emission wavelength range (400-600 nm) that does not overlap with heating-caused emission, thereby simplifying the measurement process while maintaining accuracy

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Illumination intensity

If copper-containing lithium triborate is used as thermoluminescent material, then emission intensity is improved, but emission intensity is still insufficient and requires resin binders that absorb thermoluminescence

Engineering Contradiction:
Improveemission intensityVSAvoidthermoluminescence absorption
Core Design Contradiction:
Illumination intensityVSLoss of energy

Solution Approach 1:

The patent uses copper-containing lithium heptaborate as a composite material that combines high emission intensity with appropriate optical properties, achieving both improved emission intensity and reduced absorption by resin binders compared to previous materials

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the material composition from copper-containing lithium triborate to copper-containing lithium heptaborate, which fundamentally alters the optical properties and emission characteristics to achieve higher emission intensity with lower resin absorption

Inventive Principle:
Principle #35Parameter changes

3Measurement precision

If thermoluminescent material with high emission intensity is used, then measurement accuracy is improved, but heat resistance becomes insufficient requiring complex corrections

Engineering Contradiction:
Improvedose measurement accuracyVSAvoidheat resistance
Core Design Contradiction:
Measurement precisionVSTemperature

Solution Approach 1:

The patent changes the thermal properties of the thermoluminescent material by selecting copper-containing lithium heptaborate which maintains high emission intensity while providing sufficient heat resistance to withstand the heating process without requiring complex corrections

Inventive Principle:
Principle #35Parameter changes

4Reliability

If conventional thermoluminescent materials are used, then dosimeter function is achieved, but binder absorption of thermoluminescence requires complex corrections

Engineering Contradiction:
Improvedosimeter functionVSAvoidcorrection complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent changes the optical parameters of the thermoluminescent material by using copper-containing lithium heptaborate with emission in the 400-600 nm range, which reduces absorption by epoxy resin binders, thereby maintaining dosimeter function while eliminating the need for complex corrections

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The thermoluminescent phosphor provides high emission intensity in a visible range, resistant to heat, allowing accurate three-dimensional dose distribution measurement without complex corrections and binder absorption, ensuring tissue equivalence and effective dosimeter performance.

Implementation Method 1

a thermoluminescent phosphor comprising copper-containing lithium heptaborate... the distribution of the emission intensity of thermoluminescence versus wavelength is a sole and monomodal distribution and is present in a visible range of wavelengths shorter than 600 nm

Methodology Applied
Scientific EffectThermoluminescence: Thermoluminescence

Data Source

PatentEP2612893B1Thermofluorescent material and process for producing same
Publication Date: 2016.08.10 RIKKYO GAKUIN
  • EP2612893B1 patent drawingFigure 1
  • EP2612893B1 patent drawingFigure 2(A)~2(B)
  • EP2612893B1 patent drawingFigure 3(A)~4(B)

AI summary

There is provided a thermoluminescent phosphor characterized in that a distribution of the emission intensity of thermoluminescence is present in a visible range that does not overlap the peak of the heating-caused emission intensity of the thermoluminescent phosphor itself and also has one peak within a temperature range in which a resin to be used as a binder can resist heat optically. There is also provided a method of producing the thermoluminescent phosphor. More specifically, there are provided a thermoluminescent phosphor that comprises lithium heptaborate as a base material and copper as a luminescent center present in the base material and which is characterized in that the distribution of the emission intensity of thermoluminescence versus temperature is a sole and monomodal distribution within the range of from 45°C to 130°C, and a method of producing the thermoluminescent phosphor.