Layered Copper Oxide Cathode for Sodium-Ion Battery Energy Density

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Solution Overview

Problem

Current sodium-ion batteries face limitations in energy density and stability due to the scarcity and toxicity of vanadium resources, as well as the instability and low capacity of existing cathode materials, particularly the P2-phase oxides, which restrict their practical application in large-scale energy storage systems.

Innovation Solution

A layered copper-containing oxide material with a general chemical formula Na0.68+a Ni b Cu c M d Mn e O2+δ is developed, featuring a simple preparation process and abundant raw materials, which is applied as a positive electrode active material in sodium-ion secondary batteries, providing high working voltage, initial Coulombic efficiency, and cycling stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If vanadium-based cathode materials (Na3V2(PO4)3, Na3V2(PO4)2F3) are used to achieve high voltage and capacity, then energy density is improved, but resource scarcity and toxicity increase costs and environmental harm

Engineering Contradiction:
Improveenergy densityVSAvoidtoxicity and resource scarcity
Core Design Contradiction:
Use of energy by moving objectVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical composition parameters by substituting vanadium with copper and adjusting the Na/Mn/Ni/Cu ratios to achieve high-voltage stability without toxic vanadium. The general formula Na0.68+aNibCucMdMneO2+δ allows systematic parameter optimization to maintain energy density while eliminating harmful elements.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces expensive and toxic vanadium-based materials with cheaper, abundant copper-containing materials. The copper-based cathode provides comparable performance at lower cost and without the environmental toxicity associated with vanadium extraction and processing.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Quantity of substance

If P2-phase oxide materials are used to achieve large capacity, then capacity is improved, but air stability deteriorates

Engineering Contradiction:
ImprovecapacityVSAvoidair stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent creates a composite cathode material combining multiple elements (Na, Mn, Ni, Cu) in a layered P2-phase structure. This composite approach leverages the high capacity of P2-phase oxides while the specific Cu-containing composition provides enhanced air stability compared to conventional P2-phase materials.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent introduces copper at specific compositional positions within the layered oxide structure to locally enhance stability. The general formula Na0.68+aNibCucMdMneO2+δ allows copper to occupy specific transition metal sites, providing localized stabilization that preserves overall air stability while maintaining high capacity.

Inventive Principle:
Principle #3Local quality

3Use of energy by moving object

If lithium-ion batteries are used to achieve high specific energy, then energy efficiency is improved, but resource cost increases

Engineering Contradiction:
Improvespecific energyVSAvoidresource cost
Core Design Contradiction:
Use of energy by moving objectVSQuantity of substance

Solution Approach 1:

The patent replaces lithium-ion technology with sodium-ion technology, substituting expensive and geographically concentrated lithium resources with abundant, cheap sodium resources. The copper-containing cathode material enables sodium-ion batteries to achieve competitive specific energy without the high resource costs of lithium.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent changes the electrochemical system parameters by transitioning from lithium to sodium ions and optimizing the cathode composition (Na0.68+aNibCucMdMneO2+δ) to achieve high voltage and capacity. This parameter change enables cost-effective large-scale energy storage while maintaining high specific energy performance.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentEP3021386B1Layered oxide material containing copper, and preparation method and use thereof
Publication Date: 2019.08.07 INSTITUTE OF PHYSICS CHINESE ACADEMY OF SCIENCES
  • EP3021386B1 patent drawingFigure 1~2
  • EP3021386B1 patent drawingFigure 3
  • EP3021386B1 patent drawingFigure 4

AI summary

The present invention discloses a layered copper-containing oxide material and a preparation process and purpose thereof. The material has a general chemical formula of Na0.68+aNibCucMdMncO2+δ, where Ni, Cu, M, and Mn respectively form octahedral structures together with six oxygen atoms that are most adjacent thereto, the octahedral structures have arrangements with common edges and constitute transition metal layers; alkali metal ions Na+ are located between every two of the transition metal layers; M is specifically one or more of Mg2+, Mn2+, Zn2+, Co2+, Al3+, B3+, Cr3+, Mn3+, Co3+, V3+, Zr4+, Ti4+, Sn4+, Mo4+, Ru4+, Nb4+, Sb5+, Nb5+, Mo6+, and Te6+; and a, b, c, d, e, δ, and m meet (0.68+a)+2(b+c)+md+4e=2(2+δ), and b+c+d+e=1.