Unconventional Core Resaturation via Porous Plug Mediator

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

The analysis of unconventional core samples is hindered by the loss of formation fluids during transportation to the surface, leading to non-representative measurements, and existing resaturation methods are inadequate due to high capillary pressure in small pores.

Innovation Solution

An apparatus and workflow for resaturating unconventional core samples with formation fluids at high pressures, combined with petrophysical analysis using 2D NMR T1-T2 experiments, to accurately characterize the core sample and reservoir rock properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If high pressure resaturation is used to overcome capillary pressure in small pores, then fluid saturation is improved, but equipment complexity and operational difficulty increase

Engineering Contradiction:
Improvefluid saturationVSAvoidequipment complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

A porous plug is introduced as an intermediary component between the core sample and the resaturation system. The porous plug has pore sizes larger than the core sample pores, allowing it to be saturated at lower pressures while still enabling fluid to enter the core sample's small pores through capillary action, thus mediating the high pressure requirement

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent replaces direct high-pressure mechanical injection into the core sample with a two-stage process: first saturating the porous plug at lower pressure, then allowing capillary forces to drive fluid into the core sample. This substitutes direct mechanical forcing with a combination of lower-pressure mechanics and capillary action

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Device complexity

If conventional low pressure resaturation methods are used, then equipment complexity is reduced, but fluid saturation of small pores is insufficient

Engineering Contradiction:
Improveequipment complexityVSAvoidfluid saturation
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The porous plug acts as an intermediary that can be saturated at conventional low pressures, then serves as a fluid source that delivers saturation to the core sample through capillary action, enabling low-pressure equipment to achieve high-pressure resaturation results

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the pore size parameter of the saturation medium by using a porous plug with larger pores than the core sample. This parameter change allows the plug to be saturated at lower pressures while still enabling fluid transfer to the smaller pores of the core sample through capillary pressure gradients

Inventive Principle:
Principle #35Parameter changes

3Measurement precision

If formation fluids are lost during transportation, then measurement accuracy deteriorates, but resaturation procedures are needed to restore in-situ conditions

Engineering Contradiction:
Improvemeasurement accuracyVSAvoidresaturation procedure complexity
Core Design Contradiction:
Measurement precisionVSEase of manufacture

Solution Approach 1:

The core sample is saturated with formation fluids before transportation and analysis. This preliminary saturation action ensures that the sample is in its in-situ fluid state during measurements, eliminating the need for post-transportation resaturation procedures and maintaining measurement accuracy

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies a coating or protective treatment to the core sample before transportation to prevent fluid loss. This beforehand cushioning protects the sample from the harmful effect of fluid depletion during transport, maintaining its in-situ fluid content for accurate measurements

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables representative analysis of unconventional core samples by effectively resaturating them with formation fluids at in-situ conditions, allowing for accurate determination of petrophysical properties and improved characterization of tight hydrocarbon reservoirs.

Implementation Method 1

the high capillary pressure of the core sample due to the presence of relatively small pores. Therefore, routine core resaturation methods at low pressures, such as centrifuge-based techniques used for conventional cores, are inadequate to introduce the formation fluid into the small pores of the unconventional core sample

Methodology Applied
Scientific EffectCapillary pressure: Capillary Pressure

Implementation Method 2

Nuclear magnetic resonance (NMR) core analysis applications have been shown to be useful for the characterization of fluids in shale formations

Methodology Applied
Scientific EffectNuclear magnetic resonance:

Data Source

PatentUS10466186B2Workflow for resaturation and analysis of unconventional core samples
Publication Date: 2019.11.05 SCHLUMBERGER TECH CORP
  • US10466186B2 patent drawing
  • US10466186B2 patent drawing
  • US10466186B2 patent drawing

AI summary

A method for testing an unconventional core sample is provided. The method involves loading the unconventional core sample into a sample holder and introducing fluid into the sample holder at an elevated pressure such that fluid is injected into the internal pore space of the unconventional core sample in order to resaturate the unconventional core sample with the fluid, wherein the fluid is selected from the group including a hydrocarbon fluid and a water-based formation fluid. An apparatus and a system used in combination with the method are also provided.