Core-Shell Polyester Toner for Low Melting and Stable Charge

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Solution Overview

Problem

Polyester-based toners with crystalline components exhibit lower charge and charge maintainability due to high resistivity and cohesion issues when coalesced above the crystalline resin's melting point, affecting print quality and humidity sensitivity.

Innovation Solution

An emulsion aggregation polyester toner with a core composed of amorphous and crystalline polyester and a shell of amorphous polyester, substantially free of crystalline polyester, is developed to achieve low melting temperature and stable xerographic charging across various ambient environments.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If crystalline polyester is added to lower the melting point of the toner, then the melting temperature is reduced, but the charge and charge maintainability deteriorate due to high resistivity

Engineering Contradiction:
Improvemelting temperatureVSAvoidcharge maintainability
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The toner particle is segmented into a core region containing crystalline polyester and an outer shell region containing amorphous polyester. This segmentation allows the crystalline polyester to provide low melting temperature in the core while the amorphous polyester shell provides good charge maintainability and resistivity, resolving the contradiction between melting point reduction and charge stability.

Inventive Principle:
Principle #1Segmentation

2Temperature

If crystalline polyester is added to lower the melting point, then the melting temperature is reduced, but the cohesion increases when coalesced above the melting point

Engineering Contradiction:
Improvemelting temperatureVSAvoidcohesion
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The toner particle is segmented into a core region containing crystalline polyester and an outer shell region containing amorphous polyester. The amorphous polyester shell acts as a cohesive control layer that prevents excessive adhesion between particles when coalesced above the melting point, while the crystalline core provides the desired low melting temperature.

Inventive Principle:
Principle #1Segmentation

3Temperature

If polyester-based toner is used, then the melting temperature is low, but the charge is reduced due to hydrophilic nature

Engineering Contradiction:
Improvemelting temperatureVSAvoidcharge
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The toner uses a composite structure combining crystalline polyester (for low melting point) and amorphous polyester (for good charge properties). This composite material approach allows the toner to simultaneously achieve low melting temperature and adequate charge, overcoming the inherent hydrophilic limitation of pure polyester-based toners.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The toner composition maintains excellent print quality and achieves a relative humidity sensitivity ratio close to unity in all environments, addressing the issues of charge and cohesion associated with crystalline polyester use.

Implementation Method 1

Ultra low melt particles typically display a melting point of from about 50° C. to about 100° C.

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 2

the aggregated toner particles may then be heated to enable coalescing/fusing, thereby achieving aggregated, fused toner particles

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 3

The aggregated toner particles may then be heated to enable coalescing/fusing, thereby achieving aggregated, fused toner particles

Methodology Applied
Scientific EffectCoalescing:

Implementation Method 4

the aggregated toner particles may then be heated to enable coalescing/fusing

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 5

The sensitivity ratio may be expressed as a ratio of a triboelectric charge of the toner developer in the C-zone to a triboelectric charge of the toner developer in the A-zone

Methodology Applied
Scientific EffectTriboelectric charge: Triboelectric Effect

Data Source

PatentUS7695884B2Toner compositions and processes
Publication Date: 2010.04.13 XEROX CORP

AI summary

An emulsion aggregation toner including a core and a shell wherein the core includes an amorphous polyester, a wax, a crystalline polyester and an optional colorant and wherein the shell includes an amorphous polyester and a wax and is substantially free of crystalline polyester.