Condensation Particle Counter Calibration System

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Solution Overview

Problem

Traditional methods for calibrating condensation particle counters are prone to errors due to low sensitivity of reference electrometers, biases in particle size distributions, and inability to calibrate nucleation efficiency independent of transport losses, leading to inaccurate detection efficiencies.

Innovation Solution

A calibration system using a container, pump, nebulizer, classifier, and particle counters that supplies test particles of known diameter, allowing for calibration without high-resolution particle classification and independent of transport losses, utilizing a reference condensation particle counter to detect 100% of the challenge aerosol and adjusting operating temperatures to achieve stable and repeatable particle size distributions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional high resolution particle classification is used for calibration, then measurement precision may be improved, but device complexity and susceptibility to errors increase

Engineering Contradiction:
Improvedetection efficiency calibration accuracyVSAvoidcalibration system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts and eliminates the high resolution particle classifier from the calibration system, replacing it with a much simpler setup using only a condensation particle counter, aerosol generator, and filter. This removal of complex classification equipment directly reduces device complexity while maintaining calibration accuracy through an alternative method based on particle concentration measurements at different temperatures.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses a reference condensation particle counter to create a reference measurement that copies the detection function needed for calibration. Instead of using complex particle classification, the system creates a reference aerosol and measures it with the CPC to establish detection efficiency, effectively copying the essential measurement function without the complex classification infrastructure.

Inventive Principle:
Principle #26Copying

2Quantity of substance

If traditional aerosol electrometer with particle classifier is used, then particle size distribution can be measured, but measurement precision deteriorates due to low sensitivity and various biases

Engineering Contradiction:
Improveparticle concentration measurementVSAvoidparticle size distribution accuracy
Core Design Contradiction:
Quantity of substanceVSMeasurement precision

Solution Approach 1:

The patent replaces the mechanical/electrical particle classification system (aerosol electrometer with classifier) with a thermal-based condensation particle counter system. The CPC uses vapor condensation on particles rather than electrical mobility classification, substituting a thermal-phase change mechanism for the electrical-mechanical classification system, thereby avoiding its sensitivity and bias issues.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the measurement parameter from electrical mobility (used in traditional classification) to particle concentration detection via condensation growth. By measuring particle concentration at different temperatures and using the temperature dependence of condensation efficiency, the system achieves accurate calibration without the measurement errors inherent in electrical mobility-based classification.

Inventive Principle:
Principle #35Parameter changes

3Measurement precision

If calibration is performed with traditional methods, then detection efficiency can be measured, but reliability decreases due to inability to separate nucleation efficiency from transport losses

Engineering Contradiction:
Improvedetection efficiency measurementVSAvoidcalibration reliability
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent segments the calibration process into distinct temperature-dependent measurements. By measuring particle detection efficiency at multiple temperatures and analyzing the temperature dependence separately from transport effects, the system can isolate and calibrate nucleation efficiency independently. This segmentation of the measurement approach allows reliable separation of the two previously confounded factors.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent introduces dynamic temperature variation as a control parameter to separate the effects of nucleation efficiency from transport losses. By dynamically changing the temperature and observing how detection efficiency responds, the system can distinguish between temperature-dependent nucleation effects and transport effects, thereby improving calibration reliability.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate and repeatable calibration of detection efficiencies at low particle concentrations, minimizing errors and skewing effects, and allowing for independent calibration of nucleation efficiency, resulting in improved accuracy and reliability.

Implementation Method 1

a nebulizer communicatively connected to the pump

Methodology Applied
Scientific EffectAtomization:

Implementation Method 2

an annular flow ion mobility classifier communicatively connected to the nebulizer

Methodology Applied
Scientific EffectIon mobility classification:

Implementation Method 3

a first condensation particle counter communicatively connected to the ion mobility classifier

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS20240167931A1Method and System for Calibrating Detection Efficiencies For Condensation Particle Counters
Publication Date: 2024.05.23 KANOMAX FMT INC
  • US20240167931A1 patent drawing
  • US20240167931A1 patent drawing
  • US20240167931A1 patent drawing

AI summary

A system, apparatus, and method for accurately calibrating the detection efficiency of condensation particle counters is disclosed. An apparatus for calibrating condensation particle counters includes a container for supplying test particles of a known and constant diameter, a pump communicatively connected to the container, a nanoparticle nebulizer communicatively connected to the pump; an ion mobility classifier communicatively connected to the nebulizer, a first condensation particle counter communicatively connected to the ion mobility classifier; and a second condensation particle counter communicatively connected to the ion mobility classifier.