Cross-Flow Cryogenic Slurry Filtration Using Stable Filter Media

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Solution Overview

Problem

Current separation technologies are ineffective, inefficient, and expensive for separating cryogenic solids from cryogenic liquids, particularly in cross-flow filtration, as existing filter media are not suitable for cryogenic temperatures and often require frequent cleaning or replacement due to solid deposition.

Innovation Solution

A cross-flow filtration method using a cryogenically-stable filter medium, such as sintered ceramics or polytetrafluoroethylene, that inhibits gas adsorption and solid deposition, and optimizes temperature-induced expansion and contraction to prevent damage and facilitate self-cleaning, allowing for the thickening of cryogenic slurries by tangentially passing the slurry across the filter medium.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional filter media are used for cryogenic slurry filtration, then the filtration process can be implemented, but the filter media collects solids over time requiring frequent cleaning or replacement

Engineering Contradiction:
Improvefiltration efficiencyVSAvoiddowntime for cleaning or replacing filter media
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent applies parameter changes by modifying the physical and chemical properties of the filter medium to be cryogenically stable. This includes selecting materials with appropriate thermal expansion coefficients, surface energies, and mechanical properties that prevent solid deposition and adsorption at cryogenic temperatures, thereby eliminating the need for frequent cleaning or replacement while maintaining continuous filtration productivity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent avoids the disposable approach by implementing a durable, long-lasting filter medium designed specifically for cryogenic service. Instead of using conventional media that require frequent replacement, the invention employs specialized materials that maintain their filtering capability indefinitely under cryogenic conditions, reducing both replacement costs and operational downtime

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Reliability

If filter media is selected to prevent solid adsorption, then solids can be filtered effectively, but the filter media must be tested extensively in laboratories to find the ideal material

Engineering Contradiction:
Improvefilter media performanceVSAvoidtesting and selection process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent resolves the testing complexity by establishing specific material parameter criteria for cryogenic filter media. By defining required properties such as thermal stability, surface energy characteristics, and mechanical strength at cryogenic temperatures, the invention provides a systematic selection framework that reduces extensive laboratory testing to targeted evaluation of materials meeting these specified parameters

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite materials that combine multiple properties in a single filter medium structure. These composites integrate materials with complementary characteristics - such as combining ceramic matrices with metallic or polymeric components - to achieve both chemical inertness and mechanical durability at cryogenic temperatures, thereby ensuring reliable performance without requiring complex multi-stage testing protocols

Inventive Principle:
Principle #40Composite materials

3Productivity

If existing filter media are used at cryogenic temperatures, then the filtration can proceed, but the filter media experiences temperature-change induced expansion and contraction causing damage

Engineering Contradiction:
Improvecontinuous filtration operationVSAvoidfilter media structural integrity
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The patent addresses thermal stress damage by selecting filter media materials with thermal expansion coefficients matched to their support structures and housing. This parameter matching ensures that during cryogenic cycling, all components expand and contract uniformly, preventing differential stress, delamination, or structural failure that would compromise filter integrity and require shutdown for replacement

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent explicitly accounts for thermal expansion effects by designing the filter assembly with expansion compensation mechanisms. This includes using materials with known, predictable expansion characteristics and incorporating design features such as flexible connections, expansion joints, or pre-stressed structures that accommodate dimensional changes during temperature cycling without causing damage to the filter medium or supporting infrastructure

Inventive Principle:
Principle #37Thermal expansion

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method effectively separates cryogenic liquids from solids, preventing fouling and maintaining filter integrity, thereby enhancing the efficiency and durability of the separation process while reducing maintenance costs.

Implementation Method 1

Cross-flow filtration, sometimes referred to as tangential filtration, is a common method for removing solids in reverse osmosis, nanofiltration, ultrafiltration, and microfiltration

Methodology Applied
Scientific EffectCross-flow filtration: Filter (physical)

Implementation Method 2

temperature-change induced expansion and contraction of the filter medium is optimized

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Implementation Method 3

adsorption of gases is inhibited

Methodology Applied
Scientific EffectAdsorption inhibition: Adsorption

Data Source

PatentUS10533796B2Method for thickening a cryogenic slurry using a cross-flow filter
Publication Date: 2020.01.14 U S BANK TRUST CO NAT ASSOC
  • US10533796B2 patent drawing
  • US10533796B2 patent drawing
  • US10533796B2 patent drawing

AI summary

A method for thickening a cryogenic slurry is disclosed. The method comprises providing a cryogenic slurry flow path, a cryogenic liquid discharge path, and a filter medium between the cryogenic slurry flow path and the cryogenic liquid discharge path. The cryogenic slurry comprises a solid and a cryogenic liquid. The cryogenic slurry is fed into the cryogenic slurry flow path, generally tangential to the filter medium. This causes a portion of the cryogenic liquid to cross the filter medium into the cryogenic liquid discharge path as a cryogenic liquid discharge and the cryogenic slurry to thicken to produce a thickened slurry. The filter medium comprises a cryogenically-stable material such that adsorption of gases is inhibited, deposition of solids is prevented, and temperature-change induced expansion and contraction of the filter medium is optimized.