Cross-Flow Mass Transfer Column Liquid Distributor Design

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing cross-flow packed columns have a narrow range of stable operation and inefficient mass transfer due to design limitations, leading to reduced performance when vapor and liquid flow rates deviate from optimal conditions, and excessive complexity in structural design.

Innovation Solution

The design incorporates a liquid distributor with parts A, B, and C, allowing for adjustable liquid phase flow distribution across cross-flow packing sections, enabling flexible operation from minimum to maximum reflux flow rates and preventing gas phase bypass, while maintaining high mass transfer efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If traditional cross-flow packing columns are used, then the structure is relatively simple, but the stable operation range is narrow and mass transfer efficiency decreases when flow rates deviate from optimal conditions

Engineering Contradiction:
Improvestable operation rangeVSAvoidstructural design complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The liquid distributor is divided into multiple levels with each level containing distribution nozzles arranged in specific patterns. This segmentation allows different regions of the packing to receive optimized liquid distribution, extending the stable operation range while maintaining manageable structural complexity through modular design

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The liquid distributor design enables dynamic adaptation to varying flow rates through its multi-level nozzle arrangement. As flow rates change, different levels and nozzle patterns become active, allowing the system to maintain efficient mass transfer across a broad range of operating conditions without requiring complex control mechanisms

Inventive Principle:
Principle #15Dynamics

2Productivity

If cross-flow packing sections are used, then gas phase flow is improved, but liquid phase distribution becomes uneven leading to reduced mass transfer efficiency

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidliquid phase distribution uniformity
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

Different levels of the liquid distributor have nozzles positioned at different locations and orientations tailored to specific packing sections. This local optimization ensures uniform liquid distribution across each local region, preventing channeling and maintaining high mass transfer efficiency throughout the entire column

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The liquid distributor acts as an intermediary device between the liquid feed and the packing sections. Its multi-level nozzle system mediates the liquid flow, breaking up uneven distribution patterns and ensuring homogeneous liquid-phase contact with the gas phase across all packing sections

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If the column operates at high vapor flow rates, then mass transfer increases, but liquid phase falls through slots without adequate contacting

Engineering Contradiction:
Improvemass transfer rateVSAvoidliquid-vapour contact reliability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The liquid distributor pre-distributes liquid uniformly across the packing surface before the vapor-liquid contact occurs. This preliminary action ensures that even at high vapor flow rates, liquid is already in position and properly distributed, preventing it from falling through slots without adequate contact and maintaining reliable mass transfer

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design extends the stable operation range of the mass transfer column from 5% to 100% reflux flow rates, ensuring consistent performance across varying conditions and enhancing fractionation efficiency by optimizing liquid and gas flow patterns.

Implementation Method 1

liquid distributors between the adjacent sections of the cross-flow packing and above the upper section of the cross-flow packing

Methodology Applied
Scientific EffectFluid flow distribution:

Implementation Method 2

cross-flow packing sections limited on two opposite sides by continuous side walls and separated heightwise by horizontal baffles... mass transfer occurs between vertically descending liquid phase film streaming down packing 2 and horizontally passing vapour phase flow

Methodology Applied
Scientific EffectMass transfer: Diffusion

Implementation Method 3

horizontal baffles having, successively, in the direction of gas phase, in the normal shell cross section, a window for the gas flowing on the cross-flow packing section inlet side and a continuous area with manholes on the cross-flow packing section outlet side

Methodology Applied
Scientific EffectGas flow direction:

Data Source

PatentUS10350510B2Mass transfer column of cross flow of liquid and gas (vapour) phases
Publication Date: 2019.07.16 MNUSHKIN IGOR ANATOLEVICH
  • US10350510B2 patent drawing
  • US10350510B2 patent drawing
  • US10350510B2 patent drawing

AI summary

What is described relates to cross-flow packing heat and mass transfer column vessels, where rectifying separation of liquid-vapor mixtures, distillation of liquid-vapor mixtures, and absorptive separation of liquid-vapor mixtures occur, and may be used in oil-refining, petrochemical, chemical, gas, food, and other industries. The proposed mass transfer column with cross flow of liquid and gas (vapor) phases includes shell, feed nozzle, distillate and residue withdrawal nozzles, nozzles of injection and withdrawal of auxiliary flows, cross-flow packing sections separated heightwise by horizontal baffles having, successively, in direction of gas (vapor) phase, in normal shell cross section, a window for gas (vapor) flowing on packing section inlet side and continuous area on packing section outlet side, which alternate on horizontal baffles neighboring by height, with liquid distributors between packing adjacent sections and above packing upper section, which consist of three successively mating parts: horizontal leaf, set of steps, and blind pocket.