Crosslinked Polymer Solid Electrolytes for Safer Li-Ion Cells

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Solution Overview

Problem

Lithium-ion batteries face safety concerns due to the use of flammable solvents, which can lead to accidents such as fires and explosions during overcharging or short-circuiting, necessitating the development of safer and more stable solid electrolyte materials.

Innovation Solution

The development of polymer solid electrolytes with urea or carbamate functional groups that enhance mechanical and electrochemical properties, including high ionic conductivity, tensile strength, and decomposition voltage, achieved through crosslinking reactions and the use of specific polymer structures and plasticizers, allowing for safer and more efficient lithium-ion batteries.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If flammable solvents (carbonate/ether) are used in lithium-ion batteries, then ionic conductivity and electrochemical performance are improved, but safety deteriorates due to fire and explosion risks during overcharging or short-circuiting

Engineering Contradiction:
ImprovesafetyVSAvoidflammability risk
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the physical state of the electrolyte from liquid to solid polymer form, fundamentally altering the safety parameters while maintaining ionic conductivity through careful selection of polymer matrices (PEO, PANI, PPy) and electrolyte compositions

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite polymer electrolyte systems combining multiple polymer components (e.g., PEO with PANI, or PPy with lithium salts) to achieve both high ionic conductivity and enhanced mechanical strength, eliminating flammable solvents while maintaining electrochemical performance

Inventive Principle:
Principle #40Composite materials

2Object-generated harmful factors

If solid polymer electrolytes are developed to eliminate flammable solvents, then safety is improved, but ionic conductivity and electrochemical performance may deteriorate

Engineering Contradiction:
Improveflammability riskVSAvoidionic conductivity
Core Design Contradiction:
Object-generated harmful factorsVSReliability

Solution Approach 1:

The patent optimizes parameters such as polymer molecular weight, crosslinking density, lithium salt concentration, and plasticizer content to achieve the optimal balance between mechanical strength and ionic conductivity in solid polymer electrolytes

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention introduces plasticizers (e.g., succinonitrile, ethylene carbonate) as intermediary substances that facilitate ion transport between polymer chains, enhancing ionic conductivity without compromising the solid-state safety benefits

Inventive Principle:
Principle #24Intermediary (Mediator)

3Strength

If polymer solid electrolytes with crosslinking structures are used to enhance mechanical strength, then tensile strength and stability are improved, but manufacturing complexity increases

Engineering Contradiction:
Improvetensile strengthVSAvoidmanufacturing process complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent incorporates crosslinkable functional groups (epoxy, vinyl, or isocyanate groups) into the polymer structure during synthesis, allowing crosslinking to occur in-situ during battery assembly or initial charging cycles, rather than requiring separate complex crosslinking equipment

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention employs self-crosslinking mechanisms where the polymer electrolyte undergoes crosslinking reactions autonomously under battery operating conditions (temperature, humidity, or electrical bias), eliminating the need for external crosslinking equipment and simplifying manufacturing

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The polymer solid electrolytes exhibit improved ionic conductivity, mechanical strength, and stability, leading to safer and longer-life lithium-ion batteries with enhanced charging/discharging rates and higher voltage capabilities, while eliminating the risks associated with flammable solvents.

Implementation Method 1

a polymer comprising a product of a crosslinking reaction including a polymer selected from the group consisting of

Methodology Applied
Scientific EffectCrosslinking reaction: Chemical Bonding

Implementation Method 2

various polymer solid electrolyte materials suitable for electrochemical devices such as batteries, capacitors, sensors

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Data Source

PatentEP3651253B1Polymer solid electrolyte, method of making the same, and electrochemical cell
Publication Date: 2024.02.14 FACTORIAL INC
  • EP3651253B1 patent drawingFigure 1
  • EP3651253B1 patent drawingFigure 2
  • EP3651253B1 patent drawingFigure 3A~3G

AI summary

The present invention generally relates to various polymer solid electrolyte materials suitable for various electrochemical devices and method of making the same. Certain embodiments of the invention are generally directed to solid electrolytes having relatively high ionic conductivity and other mechanical or electrical properties, e.g., tensile strength or decomposition potential. Certain aspects include a polymer, a plasticizer, and an electrolyte salt. In some cases, the polymer may exhibit certain structures such as: ,where R1 can be one of the following groups: where n is an integer between 1 and 10000, m is a integer between 1 and 5000, and R2 to R6 can each independently be one of the following structures: