Crosslinked UHMW PE Sintering Process for Orthopedic Implants

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Ultrahigh molecular weight polyethylene (UHMW PE) is difficult to process due to its intractability above its crystalline melting temperature, leading to retained morphology and increased wear and failure in applications like artificial implants, and existing methods are cumbersome, time-consuming, and negatively impact other properties such as crack resistance.

Innovation Solution

A process involving compacting virgin UHMW PE to a compacted composition, followed by sintering and crosslinking, with crosslinking initiated multiple times using gamma radiation or electron beam radiation, to enhance wear resistance and maintain high crystallinity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If UHMW PE is sintered at high temperatures to improve wear resistance, then wear resistance is improved, but the polymer retains its original shape and morphology which contributes to wear and failure

Engineering Contradiction:
Improvewear resistanceVSAvoidparticle morphology retention
Core Design Contradiction:
ReliabilityVSShape

Solution Approach 1:

The patent applies crosslinking to change the fundamental parameters of UHMW PE, transforming it from a thermally softening polymer to a crosslinked network structure that maintains dimensional stability at high temperatures. This allows the material to be sintered while preventing morphology retention, thereby improving wear resistance without the detrimental shape retention effect

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure by forming crosslinks within the UHMW PE matrix, effectively creating a new material system with combined properties: the inherent wear resistance and toughness of UHMW PE plus the thermal stability and dimensional control of crosslinked networks

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If conventional sintering processes are used to process UHMW PE, then the material can be formed, but the processes are time-consuming and negatively influence crack resistance

Engineering Contradiction:
ImproveprocessabilityVSAvoidcrack resistance
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent incorporates crosslinking agents during the compaction or sintering process, performing the crosslinking action preliminarily rather than requiring separate post-processing steps. This preliminary crosslinking improves crack resistance while maintaining efficient processing, eliminating the need for time-consuming conventional multi-step processes

Inventive Principle:
Principle #10Preliminary action

3Reliability

If UHMW PE is processed multiple times to reduce wear, then wear resistance may be improved, but the process becomes cumbersome and time-consuming

Engineering Contradiction:
Improvewear resistanceVSAvoidprocessing time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent merges the compaction, sintering, and crosslinking steps into a single integrated process sequence. By incorporating crosslinking agents and performing crosslinking during or after sintering in one continuous operation, the patent eliminates the need for multiple separate processing cycles, thereby reducing processing time while achieving improved wear resistance

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process improves wear resistance and impact strength while minimizing the negative effects on crack propagation resistance, resulting in improved performance for applications like orthopedic implants.

Implementation Method 1

crosslinking initiated multiple times using gamma radiation or electron beam radiation

Methodology Applied
Scientific EffectGamma radiation: Radiation

Implementation Method 2

crosslinking initiated multiple times using gamma radiation or electron beam radiation

Methodology Applied
Scientific EffectElectron beam radiation: Electron Beam

Implementation Method 3

sintering said compacted composition

Methodology Applied
Scientific EffectSintering: Sintering

Data Source

PatentEP2083981B1Processes comprising crosslinking polyethylene or using crosslinked polyethylene
Publication Date: 2021.10.06 SMITH & NEPHEW ORTHOPAEDICS
  • EP2083981B1 patent drawingFigure 1
  • EP2083981B1 patent drawingFigure 2
  • EP2083981B1 patent drawingFigure 3

AI summary

Provided are processes comprising crosslinking polyethylene or using crosslinked polyethylene. Furthermore, the processes may include compacting and/or sintering the polyethylene.