Crosslinked Oxidized Xanthan Acidizing Fluid Deep Penetration

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Solution Overview

Problem

Conventional acidizing fluids for subterranean formations face challenges such as limited deep penetration due to rapid spending and the use of synthetic polymers that leave undesirable residues, while natural biopolymers like xanthan have struggled with crosslinking and stability issues.

Innovation Solution

The use of in-situ crosslinked spent acids and crosslinked live acids comprising derivatized xanthan, which acts as a gelling agent to enhance penetration and prevent residue formation, along with optional base fluids and additives for improved performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional acidizing fluids with high acid strength are used, then the acid reacts quickly with formation materials to clean damage, but the acid becomes spent before achieving deep penetration into the formation

Engineering Contradiction:
Improvedamage removal efficiencyVSAvoidpenetration depth
Core Design Contradiction:
ProductivityVSLength of moving object

Solution Approach 1:

The patent applies preliminary action by pre-crosslinking the xanthan polymer before acid injection to establish a controlled viscosity structure that will maintain acid front stability and enable deep penetration throughout the treatment process

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent changes the physical-chemical parameters of the acidizing fluid by using crosslinked xanthan to modify viscosity and gel structure, transforming the fluid from a conventional low-viscosity acid solution to a structured high-viscosity fluid that maintains pressure and enables deep penetration while controlling reaction rate

Inventive Principle:
Principle #35Parameter changes

2Length of moving object

If synthetic polymers are used to gel acidizing fluids for delayed gel effect, then the fluid can penetrate deeper, but undesirable residues are left in the formation

Engineering Contradiction:
Improvepenetration depthVSAvoidresidue formation
Core Design Contradiction:
Length of moving objectVSObject-generated harmful factors

Solution Approach 1:

The patent employs a biodegradable natural polymer (xanthan) that serves as a temporary structuring agent during the acidizing process and then naturally degrades, eliminating the need for removal operations and avoiding long-term residue problems associated with synthetic polymers

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent changes the chemical composition from synthetic polymers to natural biopolymers, fundamentally altering the degradation behavior and environmental compatibility of the gelling agent while maintaining the desired rheological properties for deep penetration

Inventive Principle:
Principle #35Parameter changes

3Object-generated harmful factors

If natural biopolymers like xanthan are used for crosslinking, then the fluid is biodegradable and leaves no residue, but crosslinking ability and stability are insufficient

Engineering Contradiction:
Improveresidue formationVSAvoidcrosslinking stability
Core Design Contradiction:
Object-generated harmful factorsVSReliability

Solution Approach 1:

The patent creates a composite system by combining natural xanthan polymer with metal ion crosslinking agents (such as calcium, zinc, or iron ions) to achieve both the biodegradability of natural polymers and the crosslinking stability required for effective acidizing fluid structure maintenance

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent introduces metal ions as intermediary crosslinking agents that bridge the hydroxyl groups of xanthan polymer chains, forming stable coordinate bonds that provide the necessary gel strength and structural stability while maintaining the natural, biodegradable character of the base polymer

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for deeper penetration and longer effective fracture lengths, reduces fluid loss, and avoids leaving residues, effectively stimulating production and dissolving damage in subterranean formations without the drawbacks of conventional acidizing fluids.

Implementation Method 1

in-situ crosslinked spent acids and crosslinked live acids comprising derivatized xanthan

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 2

crosslinked oxidized xanthan...acts as a gelling agent

Methodology Applied
Scientific EffectGel formation: Gel

Implementation Method 3

the acid reacts with the formation itself, fines and damage nearest the well bore

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 4

dissolving damage in subterranean formations

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentUS7735558B2Crosslinked acids comprising derivatized xanthan and subterranean acidizing applications
Publication Date: 2010.06.15 HALLIBURTON ENERGY SERVICES INC

AI summary

Many methods are provided herein including, in one embodiment, a method comprising: providing a fluid that comprises an acid, crosslinked oxidized xanthan, and optionally, a base fluid; placing the fluid in a well bore penetrating a subterranean formation; and allowing the fluid to acidize at least a portion of the formation or damage contained therein. In another embodiment, herein provided is a fluid for subterranean uses comprising an acid and crosslinked, oxidized xanthan.