Crosslinked Xanthan Acidizing Fluids for Deep Penetration

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Solution Overview

Problem

Conventional acidizing fluids for subterranean formations face challenges such as limited deep penetration due to rapid spending and the undesirable residues left by synthetic polymers, which hinder effective permeability enhancement and require costly remedial operations.

Innovation Solution

The use of acidizing fluids comprising in-situ crosslinked spent acids and crosslinked live acids with derivatized xanthan, which acts as a gelling agent to enhance penetration and prevent residue formation, allowing for deeper fracture acidizing lengths and reduced fluid loss.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If conventional acidizing fluids with high acid strength are used, then the acid can quickly react with formation materials near the well bore, but the acid becomes spent before achieving desirable deep penetration into the formation

Engineering Contradiction:
Improvereaction rateVSAvoidpenetration depth
Core Design Contradiction:
SpeedVSLength of moving object

Solution Approach 1:

The acidizing fluid is pre-gelled using crosslinked polymers before injection to control its flow and reaction characteristics. This preliminary gelling action allows the acid to maintain its reactive strength while moving deeper into the formation before the gel structure breaks down, enabling both rapid reaction and deep penetration.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The gel structure of the acidizing fluid is designed to be dynamic, maintaining its gel state during injection and initial flow to control penetration rate, then breaking down at the target depth to allow rapid acid reaction. This dynamic transition enables the fluid to adapt its properties during different stages of the acidizing process.

Inventive Principle:
Principle #15Dynamics

2Reliability

If synthetic polymers are used to gel acidizing fluids, then delayed gelation and temperature tolerance are achieved, but undesirable residues are left in the subterranean formation requiring costly remedial operations

Engineering Contradiction:
Improvetemperature toleranceVSAvoidresidue formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The polymer structure is chemically modified by changing its parameters - specifically using partially hydrolyzed polyacrylonitrile with controlled degrees of hydrolysis and specific molecular weights. These parameter changes enable the polymer to maintain temperature tolerance while being completely degradable into harmless substances, eliminating residue formation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a disposable, fully degradable polymer gel system that performs its function temporarily during the acidizing process and then completely breaks down. This approach replaces persistent synthetic polymers with a short-lived, environmentally benign alternative that leaves no harmful residues.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Ease of manufacture

If natural biopolymers are used in crosslinked gel acidizing applications, then degradability is achieved, but the polymers function at relatively low temperatures and have poor crosslinking ability

Engineering Contradiction:
ImprovedegradabilityVSAvoidfunctional temperature range
Core Design Contradiction:
Ease of manufactureVSTemperature

Solution Approach 1:

The patent creates a composite polymer system by combining partially hydrolyzed polyacrylonitrile chains with crosslinking agents to form a gel network. This composite structure integrates the degradability of natural polymer systems with the temperature tolerance and crosslinking capability of synthetic polymers, achieving both properties simultaneously.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The acidizing fluids achieve deeper penetration and longer effective fracture lengths, reduce residue formation, and effectively stimulate production by dissolving damage and removing fines, while minimizing fluid loss and potential for costly clean-up operations.

Implementation Method 1

crosslinked acids comprising derivatized xanthan

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 2

crosslinked live acids comprising derivatized xanthan, which acts as a gelling agent

Methodology Applied
Scientific EffectGel formation: Gel

Implementation Method 3

the acidic solution reacts with acid-soluble materials contained in the formation which results in an increase in the size of the pore spaces

Methodology Applied
Scientific EffectChemical dissolution: Solvation

Implementation Method 4

crosslinked oxidized xanthan

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentUS7754658B2Crosslinked acids comprising derivatized xanthan and subterranean acidizing applications
Publication Date: 2010.07.13 HALLIBURTON ENERGY SERVICES INC

AI summary

Many methods are provided herein including, in one embodiment, a method comprising: providing a fluid that comprises an acid, crosslinked oxidized xanthan, and optionally, a base fluid; placing the fluid in a well bore penetrating a subterranean formation; and allowing the fluid to acidize at least a portion of the formation or damage contained therein. In another embodiment, herein provided is a fluid for subterranean uses comprising an acid and crosslinked, oxidized xanthan.