Crucible Isolating Layer Spraying with Temperature Feedback

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Solution Overview

Problem

Conventional methods for manufacturing isolating layers on crucibles for silicon ingot production face challenges in achieving uniformity and desired thickness, leading to cracks and reduced quality and yield of silicon ingots due to thermal expansion differences and impurity diffusion.

Innovation Solution

A method using a temperature-sensing spraying device that adjusts the spraying parameters based on temperature differences measured before and after applying the slurry to ensure the isolating layer is within a predetermined temperature range, ensuring uniformity and thickness, thereby preventing cracks and improving ingot quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional spraying method is used to form isolating layer, then the crucible can be protected from molten silicon adhesion, but the thickness and uniformity of the isolating layer cannot be controlled, leading to cracks

Engineering Contradiction:
Improvecrucible protectionVSAvoidisolating layer thickness uniformity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent employs temperature sensing feedback during the spraying process. Temperature sensors detect the temperature of the crucible inner wall in real-time, and this information is fed back to the control system which adjusts spraying parameters (such as spraying speed, distance, or slurry flow rate) to maintain the temperature within a predetermined range, ensuring uniform isolating layer formation without cracks

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent changes the control parameter from simple spraying duration or distance to temperature-based control. By monitoring temperature changes during spraying and adjusting spraying parameters accordingly, the system achieves precise control over isolating layer thickness and uniformity, preventing crack formation

Inventive Principle:
Principle #35Parameter changes

2Duration of action of stationary object

If the isolating layer is not uniform or has cracks, then the crucible life is extended, but the silicon ingot quality and yield decrease due to impurity diffusion

Engineering Contradiction:
Improvecrucible lifeVSAvoidsilicon ingot quality
Core Design Contradiction:
Duration of action of stationary objectVSReliability

Solution Approach 1:

The temperature sensing feedback system ensures the isolating layer is formed uniformly and without defects by continuously monitoring and adjusting spraying parameters. This prevents cracks and non-uniformities that would otherwise allow impurity diffusion, thereby maintaining silicon ingot quality while extending crucible life through proper isolating layer formation

Inventive Principle:
Principle #23Feedback

3Manufacturing precision

If complicated measurement method is used to measure inner wall of crucible, then the spraying accuracy can be improved, but the manufacturing time increases significantly

Engineering Contradiction:
Improvespraying accuracyVSAvoidmeasurement time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent replaces complicated mechanical measurement systems with a temperature-based sensing system. Instead of physically measuring and mapping the crucible inner wall geometry, the system uses temperature sensors to detect the state of the inner wall during spraying, which is then used to control the spraying process. This substitution dramatically reduces measurement time while maintaining or improving spraying accuracy

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The crucible itself serves as the measurement reference by its temperature response to spraying. The temperature changes of the crucible inner wall during spraying provide real-time feedback about the isolating layer formation, eliminating the need for separate, time-consuming measurement steps. The system uses the crucible's own thermal properties as the measurement mechanism

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method effectively maintains uniformity and thickness of the isolating layer within a 6° C. to 12° C. temperature difference range, significantly reducing the crack probability of silicon ingots to 0.01% and extending crucible life, while ensuring consistent quality and yield.

Implementation Method 1

a temperature sensing unit electrically connected to the processing unit... measuring an inner wall of the crucible to get a first temperature by the temperature sensing unit; measuring the isolating layer formed on the inner wall of the crucible to get a second temperature by the temperature sensing unit

Methodology Applied
Scientific EffectTemperature sensing: Thermocouple

Implementation Method 2

heating the crucible, and then measuring an inner wall of the crucible to get a first temperature by the temperature sensing unit

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS9885125B2Method for manufacturing isolating layer onto crucible and spraying device related thereto
Publication Date: 2018.02.06 SINO AMERICAN SILICON PRODUCTS INC
  • US9885125B2 patent drawing
  • US9885125B2 patent drawing
  • US9885125B2 patent drawing

AI summary

A method for manufacturing an isolating layer onto a crucible includes the steps as follows: providing a spraying device for the following spraying steps; heating the crucible and measuring the heated crucible to get a first temperature; spraying a slurry on the inner wall of the crucible to form an isolating layer by a spraying unit with a predetermined spraying manner; measuring the isolating layer to get a second temperature; obtaining a value for the difference between the first and second temperatures and judging whether the difference value in a within predetermined difference scope or not, in which the predetermined difference scope is about 6° C.˜12° C.; when the difference value is not in the predetermined difference scope, adjusting the predetermined spraying manner; when the difference value is in the predetermined difference scope, implementing the above spraying steps to the crucible.