Cryocooler Cooling Shroud for Molecular Beam Epitaxy

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Solution Overview

Problem

Current molecular beam epitaxy (MBE) techniques require expensive cryogenic fluids for cooling surfaces inside vacuum chambers, leading to safety hazards, frequent refills, and complex piping systems, which are inefficient and pose handling risks.

Innovation Solution

An apparatus and method utilizing a cryocooler, such as a Gifford-McMahon or pulse tube cryocooler, to cool surfaces within the vacuum chamber to cryogenic temperatures, eliminating the need for cryogenic fluids by integrating a vibration damping mechanism and thermal coupling for efficient cooling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If cryogenic fluids are used to cool the shroud, then the shroud can be cooled to cryogenic temperatures for effective impurity trapping, but the system complexity increases due to required piping and storage tanks

Engineering Contradiction:
Improveshroud temperatureVSAvoidpiping and storage system
Core Design Contradiction:
TemperatureVSDevice complexity

Solution Approach 1:

The patent extracts the cryogenic fluid storage and piping system from the vacuum chamber environment. By using a cryocooler with a cold finger that extends through the chamber wall, the complex fluid handling system is moved outside the vacuum environment, eliminating the need for internal piping and storage tanks while maintaining effective cooling of the shroud to cryogenic temperatures

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The cold finger acts as an intermediary thermal connection between the external cryocooler and the internal shroud. This mediator transfers cryogenic cooling capacity across the vacuum chamber boundary without requiring direct fluid contact or complex internal piping, simplifying the overall system architecture

Inventive Principle:
Principle #24Intermediary (Mediator)

2Temperature

If cryogenic fluids are used for cooling, then effective impurity trapping is achieved, but safety hazards arise from frostbite and asphyxiation risks

Engineering Contradiction:
Improveshroud temperatureVSAvoidsafety hazards
Core Design Contradiction:
TemperatureVSObject-affected harmful factors

Solution Approach 1:

The hazardous cryogenic fluids are completely extracted from the vacuum chamber environment. The closed-cycle cryocooler operates externally, eliminating direct handling and presence of cryogenic liquids inside the chamber, thereby removing frostbite and asphyxiation hazards while maintaining the necessary cryogenic temperatures for impurity trapping

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The closed-cycle cryocooler system operates autonomously without requiring manual refilling or handling of cryogenic fluids. The system self-regulates the cooling process, eliminating human interaction with hazardous materials while maintaining effective shroud cooling for impurity removal

Inventive Principle:
Principle #25Self-service

3Quantity of substance

If cryogenic fluids are used to maintain low pressure, then impurity trapping is effective, but periodic refills are required due to boil-off

Engineering Contradiction:
Improveimpurity trapping efficiencyVSAvoidrefill frequency
Core Design Contradiction:
Quantity of substanceVSLoss of time

Solution Approach 1:

The closed-cycle cryocooler provides continuous, uninterrupted cooling operation without the periodic interruptions required by boil-off refills. The system maintains stable cryogenic temperatures indefinitely, ensuring continuous impurity trapping efficiency without time loss associated with refilling operations

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The cryocooler system is self-sufficient and self-regulating, automatically maintaining the required cooling capacity without external intervention. The closed cycle eliminates the need for periodic refilling operations, making the system autonomous and eliminating time loss associated with maintenance refills

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution effectively traps impurities on the cooling shroud surfaces, maintaining low chamber pressure without the risks and costs associated with cryogenic fluids, enhancing the efficiency and safety of the MBE process.

Implementation Method 1

A cryocooler having at least a portion extending into the vacuum chamber is operatively coupled to the cooling shroud for extracting heat therefrom, and cooling the at least one surface of the cooling shroud to cryogenic temperatures

Methodology Applied
Scientific EffectHeat extraction: Cooling

Implementation Method 2

At cryogenic temperatures, impurities condense and are trapped on the surface of the cooling shroud, reducing the pressure in the chamber. This effect is known as cryo-pumping

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

the apparatus further comprises a vibration damping mechanism attaching the cryocooler to the enclosure

Methodology Applied
Scientific EffectVibration damping: Damping

Data Source

PatentUS11015262B2Apparatus and method for molecular beam epitaxy
Publication Date: 2021.05.25 ANYON SYSTEMS INC
  • US11015262B2 patent drawing
  • US11015262B2 patent drawing
  • US11015262B2 patent drawing

AI summary

An apparatus and method for molecular beam epitaxy are described herein. The apparatus comprises an enclosure defining a vacuum chamber. A substrate holder is mounted within the vacuum chamber. At least one molecular beam source is in fluid communication with the vacuum chamber. A cooling shroud having at least one surface is mounted within the vacuum chamber spaced from the substrate holder. A cryocooler having at least a portion extending into the vacuum chamber is operatively coupled to the cooling shroud for extracting heat therefrom, and cooling the at least one surface of the cooling shroud to cryogenic temperatures.