Cryogenic Air Separation Column Layout for Compact Cold Boxes

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Solution Overview

Problem

Existing air distillation technologies face challenges in optimizing the volume usage of cold boxes and ensuring efficient liquid loading and two-phase air supply in air separation apparatuses, particularly with the placement and configuration of subcoolers and columns.

Innovation Solution

A double air separation column apparatus with a medium pressure column and a low pressure column thermally connected by a reboiler-condenser, where the subcooler is strategically placed to balance column heights and optimize the cold box volume, allowing for a compact design with corrugated-crossed structured packing and a parallel section with a height of less than 35 meters.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Volume of moving object

If the subcooler is placed below the low pressure column with traditional configurations, then the column heights can be optimized, but the cold box volume is not efficiently utilized and the overall height exceeds 35 meters

Engineering Contradiction:
Improvecold box volume utilizationVSAvoidcold box height
Core Design Contradiction:
Volume of moving objectVSLength of stationary object

Solution Approach 1:

The subcooler is repositioned from a vertical arrangement to a horizontal arrangement at ground level, changing the spatial dimension of placement. This allows the cold box to be shortened in height while maintaining adequate cooling function, achieving a height under 35 meters while efficiently utilizing the cold box volume.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If the medium pressure column is elevated, then the low pressure column can be positioned for optimal performance, but the two-phase air supply and liquid loading efficiency are compromised

Engineering Contradiction:
Improveliquid loading efficiencyVSAvoidtwo-phase air supply
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The medium pressure column is placed at ground level, creating an equipotential position that facilitates natural two-phase air supply and optimal liquid loading. This ground-level placement eliminates the need for complex pumping systems and ensures efficient operation of the distillation process.

Inventive Principle:
Principle #12Equipotentiality

3Length of stationary object

If the cold box height is reduced to under 35 meters, then the apparatus becomes more compact, but the configuration of subcooler and columns becomes more complex

Engineering Contradiction:
Improvecold box heightVSAvoidcolumn and subcooler configuration
Core Design Contradiction:
Length of stationary objectVSDevice complexity

Solution Approach 1:

The apparatus is segmented into distinct functional modules: the medium pressure column, low pressure column, subcooler, and reboiler-condenser are arranged as separate but thermally connected units. This modular segmentation allows each component to be optimized independently while maintaining an overall compact configuration under 35 meters in height.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration enhances the efficiency of air separation by ensuring good liquid loading and two-phase air supply, optimizing the cold box volume, and enabling a compact design while maintaining effective operation.

Implementation Method 1

a double column thermally connected together by a reboiler-condenser

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 2

Nitrogen from the head of the column is sent to the reboiler 5 where it condenses

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

In the subcooler, rich liquid from the vessel of the medium pressure column is cooled before being sent to the second elongated element

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 4

corrugated-crossed structured packings

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 5

corrugated-crossed structured packings

Methodology Applied
Scientific EffectConvection: Convection

Implementation Method 6

A bottom liquid 13 of column 3 is sent to the top of the auxiliary column 2 after having been pressurized in a pump p

Methodology Applied
Scientific EffectPressurization: Pressurisation

Data Source

PatentEP2132509B1Method and device for separating air by cryogenic distillation
Publication Date: 2018.06.27 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP2132509B1 patent drawingFigure 1

AI summary

The invention relates to an air separation apparatus that comprises a first member (A) having an elongated shape and including the medium-pressure column (1) of a dual column, on top of which are provided a reboiler-condenser (5) and an auxiliary column (2) containing at least one theoretical plate defining the lower portion of the low-pressure column, a second member (B) having an elongated shape and defining the rest of the low-pressure column, means (11) for supplying air from the main exchange line to the medium-pressure column and a subcooler (6) provided under the first or second member having an elongated shape, means for supplying a tank liquid from the medium-pressure column to the subcooler and then to the second member having an elongated shape and/or a means for supplying a liquid from the head of the medium-pressure column to the subcooler and then to the second member having an elongated shape, and means for supplying a gas from the head of the second member having an elongated shape to the subcooler.