Method for preparing round emulsion beads using low temperature cooling and the product thereof

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Solution Overview

Problem

Current methods for preparing emulsion beads fail to maintain their shape at room temperature without swelling or disintegration, and when applied to the skin, they can cause an unpleasant foreign substance feeling due to graininess.

Innovation Solution

A cryogenic freezing method is employed to form solid round emulsion beads by dropping liquid emulsion into a low-temperature refrigerant, which can be coated with a solid or gel-forming composition to maintain shape stability and facilitate easy disintegration into a liquid emulsion upon application.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If emulsion beads are prepared using conventional methods, then they can be easily manufactured, but they fail to maintain their shape at room temperature and cause grainy feelings on skin

Engineering Contradiction:
Improvebead shape stabilityVSAvoidgrainy feeling on skin
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The patent employs phase transition by freezing liquid emulsion droplets into solid beads using a freezing solvent. This phase change from liquid to solid state enables the beads to maintain their shape at room temperature while preventing the grainy feeling associated with conventional emulsion beads, as the solid structure provides shape stability without disintegration

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The patent changes the physical state parameter of the emulsion beads from liquid to solid through freezing. This parameter change allows the beads to maintain shape stability at room temperature and eliminates the grainy feeling on skin, while still allowing easy disintegration into liquid form upon application

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If emulsion beads are stored at room temperature, then they are convenient for use, but they swell and disintegrate losing their shape

Engineering Contradiction:
Improvestorage convenienceVSAvoidbead shape maintenance
Core Design Contradiction:
Ease of operationVSShape

Solution Approach 1:

The patent uses phase transition to create solid emulsion beads that remain stable at room temperature. The solid phase structure prevents swelling and disintegration that occur with conventional liquid emulsion beads, maintaining shape integrity during storage while still being convenient for use

Inventive Principle:
Principle #36Phase transitions

3Manufacturing precision

If liquid emulsion is dropped into freezing solvent, then solid round emulsion beads are formed, but they require low temperature storage

Engineering Contradiction:
Improvebead shape formationVSAvoidstorage temperature requirement
Core Design Contradiction:
Manufacturing precisionVSTemperature

Solution Approach 1:

The patent employs phase transition from liquid to solid through freezing to form round emulsion beads with high shape precision. The freezing process creates a solid structure that maintains its shape, and while low temperature storage is required to maintain this solid state, the shape formation precision is significantly improved compared to conventional methods

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method allows for stable storage and use of solid emulsion beads at low temperatures, which maintain shape at room temperature and disintegrate easily into a liquid without grainy feelings when applied, providing a smooth application experience.

Implementation Method 1

dropping liquid emulsion into a low-temperature refrigerant, which can be coated with a solid or gel-forming composition to maintain shape stability

Methodology Applied
Scientific EffectFreezing: Freezing

Implementation Method 2

A cryogenic freezing method is employed to form solid round emulsion beads by dropping liquid emulsion into a low-temperature refrigerant

Methodology Applied
Scientific EffectCryogenic freezing: Cryogenics

Data Source

PatentUS9662282B2Method for preparing round emulsion beads using low temperature cooling and the product thereof
Publication Date: 2017.05.30 KPT
  • US9662282B2 patent drawing
  • US9662282B2 patent drawing
  • US9662282B2 patent drawing

AI summary

The present invention relates to a method for manufacturing solid round emulsion beads by dropping liquid emulsion into a cryogenic freezing refrigerant. The obtained solid round emulsion beads can be stored and used at a low temperature. The solid round emulsion beads can be coated with a solution containing a composition which is solid at room temperature or which can form gel. The emulsion beads can be prepared by using liquid emulsion containing additional composition, which is solid at room temperature or can form gel, in the water phase of oil-in-water (O/W) emulsion or the oil phase of oil-in-water (W/O) emulsion. The emulsion beads prepared by the present invention can maintain its shape without swelling and/or damage but with stability and does not give any grainy feeling when the liquid emulsion was applied on the skin.