Cu-Co-Si Alloy Strip Multi-Stage Aging Suppresses Hanging Curl

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Solution Overview

Problem

Cu-Co-Si-based copper alloys for electronic components face challenges in achieving a balance of high strength, electrical conductivity, and spring bending elastic limit, while also experiencing issues with shape accuracy and hanging curl during industrial-scale strip production, particularly due to batch furnace aging treatments that lead to curling and reduced dimension stability.

Innovation Solution

A Cu-Co-Si-based alloy strip is produced through a method involving solution treatment followed by multi-stage aging treatment under specific temperature and time conditions, with cold rolling and thermal refining annealing, which suppresses hanging curl and enhances strength, electrical conductivity, and spring bending elastic limit, and is characterized by a diffraction intensity ratio and composition within defined ranges.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If batch furnace aging treatment is used for industrial-scale production, then production efficiency is improved, but hanging curl occurs and shape accuracy deteriorates

Engineering Contradiction:
Improveproduction efficiencyVSAvoidshape accuracy
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent applies segmentation by dividing the single-stage aging treatment into multiple stages with different temperature conditions. The first aging treatment uses a higher temperature (400-500°C) to achieve rapid precipitation hardening, while the second aging treatment uses a lower temperature (200-400°C) to refine the precipitate distribution and reduce internal stresses. This multi-stage approach segments the heat treatment process to simultaneously achieve high productivity through efficient hardening and high shape accuracy through stress reduction and curl suppression.

Inventive Principle:
Principle #1Segmentation

2Strength

If aging treatment is conducted to increase strength, then mechanical strength is improved, but spring bending elastic limit may be compromised

Engineering Contradiction:
Improvemechanical strengthVSAvoidspring bending elastic limit
Core Design Contradiction:
StrengthVSStress or pressure

Solution Approach 1:

The patent applies parameter changes by optimizing the temperature and time parameters of the aging treatment. The first aging treatment operates at 400-500°C for 1-24 hours to achieve significant strength increase through precipitate formation. The second aging treatment operates at 200-400°C for 1-24 hours to adjust the precipitate distribution and reduce internal stresses. By changing the temperature parameter between stages, the patent achieves both high mechanical strength and high spring bending elastic limit, with the alloy exhibiting 0.2% offset tensile strength of 500-800 MPa and spring bending elastic limit of 300-500 MPa.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If Cu-Co-Si alloy composition is used instead of Cu-Ni-Si alloy, then electrical conductivity is improved, but spring bending elastic limit is insufficient

Engineering Contradiction:
Improveelectrical conductivityVSAvoidspring bending elastic limit
Core Design Contradiction:
ReliabilityVSStress or pressure

Solution Approach 1:

The patent applies composite materials by creating a dual-phase microstructure consisting of a copper matrix with dispersed Co-Si intermetallic precipitates. The copper matrix provides high electrical conductivity (50-80% IACS), while the Co-Si precipitates provide strengthening and improve spring bending elastic limit. The controlled precipitation of fine Co-Si particles during the two-stage aging treatment creates a composite structure that combines the electrical conductivity benefits of Cu-Co-Si alloy with the mechanical properties needed for high spring bending elastic limit.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method results in a Cu-Co-Si-based alloy strip with improved balance of strength, electrical conductivity, and spring bending elastic limit, while effectively controlling hanging curl, ensuring enhanced shape accuracy and stability during press working.

Implementation Method 1

a supersaturated solid solution, which has been subjected to solution treatment

Methodology Applied
Scientific EffectSolution treatment: Solid Solution Strengthening

Implementation Method 2

subjected to ageing treatment, whereby fine precipitates are homogeneously dispersed and not only the strength but also the electrical conductivity of the alloy are increased

Methodology Applied
Scientific EffectPrecipitation hardening: Precipitation Hardening

Implementation Method 3

performing solution treatment at 950-1050°C, and then cooling the material temperature with an average cooling rate of at least 15°C/sec from 850°C to 400°C

Methodology Applied
Scientific EffectQuenching: Cooling

Data Source

PatentEP2692879B1Cu-co-si-based copper alloy strip for electron material, and method for manufacturing same
Publication Date: 2018.12.19 JX NIPPON MINING & METALS CORP
  • EP2692879B1 patent drawingFigure 1
  • EP2692879B1 patent drawingFigure 2
  • EP2692879B1 patent drawingFigure 3

AI summary

Cu-Co-Si-based alloy strip, which has not only an excellent balance between strength and electrical conductivity but also suppressed hanging curl, is provided. The copper alloy strip for electronic materials comprises 0.5-2.5 mass% of Co, 0.1-0.7 mass% of Si, the balance Cu and inevitable impurities, wherein, from a result obtained from measurement of an X ray diffraction pole figure, using a rolled surface as a reference plane, the following (a) is satisfied. (a) A diffraction peak height at ß angle 120° among diffraction peak intensities by ß scanning at α=25° in a {200} pole figure is at least 10 times that of standard copper powder.