Smoothed III-N Substrates Using cBN Abrasive Polishing

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Solution Overview

Problem

Existing methods for polishing III-N surfaces, particularly GaN substrates, face challenges in effectively smoothing chemically inert and hard surfaces without damaging the crystal lattice, as conventional abrasive materials like diamond cause significant damage, while softer materials like silicon oxide are inadequate for removing material from these surfaces.

Innovation Solution

The use of cubic boron nitride (cBN) as an abrasive particle material in a polishing process, which balances hardness to effectively remove material from chemically inert and hard III-N surfaces while minimizing lattice damage, combined with a water-soluble suspension containing substances like ammonia or KOH, and a multi-step process with decreasing particle sizes for enhanced efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If diamond slurry is used for polishing III-N surfaces, then material removal efficiency is improved, but crystal lattice damage increases significantly

Engineering Contradiction:
Improvematerial removal efficiencyVSAvoidcrystal lattice damage
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the key parameter of abrasive material from diamond to cubic boron nitride (cBN). This parameter change enables effective material removal from chemically inert III-N surfaces while minimizing crystal lattice damage, as cBN has appropriate hardness and chemical compatibility for this application

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses a water-soluble suspension containing cBN particles that can be easily rinsed away after polishing. This disposable suspension approach eliminates the need for complex cleaning processes and ensures complete removal of abrasive particles from the polished surface

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Object-affected harmful factors

If softer abrasive materials like silicon oxide are used, then crystal lattice damage is reduced, but material removal capability becomes inadequate for chemically inert surfaces

Engineering Contradiction:
Improvecrystal lattice damageVSAvoidmaterial removal capability
Core Design Contradiction:
Object-affected harmful factorsVSProductivity

Solution Approach 1:

The invention optimizes the hardness parameter of the abrasive material by selecting cubic boron nitride, which has intermediate hardness between diamond and softer materials like silicon oxide. This parameter optimization provides the right balance for effectively removing material from chemically inert III-N surfaces while limiting crystal damage

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If multiple polishing steps with different abrasives are used, then surface quality is improved, but process complexity increases

Engineering Contradiction:
Improvesurface qualityVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention makes the cBN-based suspension universally applicable for polishing all III-N surfaces regardless of chemical inertness or polarity. This single versatile polishing step replaces multiple specialized steps required by conventional methods, simplifying the overall process while maintaining high surface quality

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The water-soluble suspension is designed to be easily removed after polishing, eliminating the need for complex multi-step cleaning and preparation processes. This disposable approach simplifies the overall manufacturing process while achieving excellent surface results

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach achieves excellent surface smoothing with extremely low surface roughness and preserved crystal quality, demonstrated by reduced standard deviation of rms values and improved crystal quality metrics such as rocking curve and micro-Raman measurements, suitable for large-area substrates and templates.

Implementation Method 1

cubic boron nitride (cBN) is used as the abrasive particle material

Methodology Applied
Scientific EffectAbrasion: Abrasion

Implementation Method 2

a water-soluble suspension containing substances like ammonia or KOH

Methodology Applied
Scientific EffectChemical etching:

Data Source

PatentEP3157045B1Smoothed iii-n substrates
Publication Date: 2021.09.08 FREIBERGER COMPOUND MATERIALS GMBH
  • EP3157045B1 patent drawingFigure 1~2

AI summary

A described method for producing smoothed III-N, in particular smoothed III-N substrate or III-N template, where III denotes at least one element of group III of the periodic table selected from Al, Ga, and In, makes it possible to provide large-area III-N substrates or III-N templates with diameters of at least 40 mm exhibiting homogeneity and very low surface roughness across the entire substrate or wafer surface. For example, when mapping the wafer surface with a white-light interferometer, the standard deviation of the rms values ​​is 5% or less. This property is simultaneously achieved with very good crystal quality at the surface or near-surface regions, measurable, for example, by rocking curve mapping and/or micro-Raman mapping.