Curable Polymer Colorimetric Sensors for Radiation Detection

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Solution Overview

Problem

Current radiation and thermal energy sensors based on photochromic or thermochromic dyes face limitations such as limited tunability for radiation detection, the need for calibration, and potential photobleaching, making them inadequate for certain applications.

Innovation Solution

Multi-layered colorimetric sensors utilizing a curable layer with functionalized polymers and polymerizable monomers that change optical properties upon exposure to radiation or thermal energy, allowing for versatile detection without the limitations of photochromic or thermochromic dyes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If photochromic or thermochromic dyes are used in colorimetric sensors, then the sensors can detect radiation or thermal energy through color change, but the response has limited tunability and requires calibration

Engineering Contradiction:
Improvedetection accuracyVSAvoidtunability
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent changes the chemical parameters of the sensing material from photochromic/thermochromic dyes to curable polymer compositions. By adjusting polymer composition, crosslinking density, and curing conditions, the sensor response can be tuned across different radiation and thermal energy ranges without requiring calibration, thus improving both measurement precision and adaptability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite curable layer compositions containing multiple polymers, photoinitiators, and functional additives. This composite approach enables independent optimization of different properties: base polymers provide structural integrity, photoinitiators control curing response, and functional additives enhance specific detection capabilities, achieving both precision and tunability simultaneously

Inventive Principle:
Principle #40Composite materials

2Reliability

If photochromic dyes are used in colorimetric sensors, then the sensors can provide color change response, but photobleaching occurs reducing durability

Engineering Contradiction:
Improveresponse permanenceVSAvoidsensor lifespan
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent replaces expensive, long-lived but photobleaching-prone photochromic dyes with cheaper, permanently responsive curable polymer systems. The curable polymers undergo irreversible chemical changes upon exposure, eliminating photobleaching and extending sensor lifespan while maintaining reliable response permanence

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent substitutes the reversible physical chemistry of photochromic dyes with the irreversible chemical crosslinking of curable polymers. This chemical mechanism substitution eliminates the photobleaching limitation inherent in dye-based systems, providing permanent, non-fading responses that enhance both reliability and duration

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Ease of operation

If photochromic or thermochromic dyes are used in colorimetric sensors, then the sensors can detect radiation or thermal energy, but calibration and correlation steps are necessary

Engineering Contradiction:
Improvesensor usabilityVSAvoidcalibration time
Core Design Contradiction:
Ease of operationVSLoss of time

Solution Approach 1:

The patent incorporates calibration-free sensor response characteristics into the curable polymer formulation itself. The polymer composition and crosslinking chemistry are pre-engineered to provide direct, linear responses to radiation and thermal energy exposure, eliminating the need for separate calibration and correlation steps and reducing operational time

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The curable polymer sensors are designed to be self-calibrating through their inherent chemical response mechanisms. The polymerization and crosslinking reactions automatically produce consistent, reproducible optical changes that directly correlate with exposure levels without requiring external calibration procedures, thereby improving ease of operation and eliminating time loss

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

These sensors provide fast, permanent responses and can detect exposure to radiation or thermal energy with improved tunability and durability, eliminating the need for calibration and reducing the risk of photobleaching, enabling more accurate and reliable measurements.

Implementation Method 1

a curable layer over the reflective surface, the curable layer comprising a functionalized polymer having at least one polymerizable functional group thereon... upon exposure to (i) a threshold amount of radiation

Methodology Applied
Scientific EffectPhotopolymerization: Photopolymerisation

Implementation Method 2

a reflective surface on the support substrate... capable of a change in one or more optical properties upon exposure to radiation or thermal energy

Methodology Applied
Scientific EffectReflection: Reflection

Data Source

PatentEP2035794B1Colorimetric sensors, array of sensors, sensor device and method of detecting radiation or thermal energy
Publication Date: 2020.05.06 3M INNOVATIVE PROPERTIES CO
  • EP2035794B1 patent drawingFigure 1~2
  • EP2035794B1 patent drawingFigure 3~4F
  • EP2035794B1 patent drawingFigure 5A~5B

AI summary

Colorimetric sensors comprising a reflective surface and a curable layer are disclosed. Devices comprising the colorimetric sensors and methods of making the sensors and devices are also disclosed. Methods of using the sensors and devices in numerous applications are also disclosed.