CVD Reactor Ceiling Temperature Control via Purge Gas

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Solution Overview

Problem

Conventional CVD reactors face challenges in maintaining a uniform temperature profile across the process chamber ceiling due to local variations in gap height, leading to inconsistent energy flux and differing reaction rates, resulting in qualitatively different layer deposition on substrates.

Innovation Solution

The method involves measuring temperatures at multiple azimuthal positions around the central axis of the process chamber ceiling, using pyrometers to determine an average and difference value, which adjusts the purge gas composition to regulate thermal resistance in the gap space, allowing for precise control of the process chamber ceiling temperature and local corrections to gap height.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the temperature of the process chamber ceiling is determined at only one arbitrary point, then the measurement is simple, but the temperature control precision is poor and does not reflect the actual average temperature

Engineering Contradiction:
Improvetemperature measurement precisionVSAvoidtemperature measurement system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The process chamber ceiling temperature measurement is segmented into multiple azimuthal positions (at least two, preferably three or more) around the central axis. Each position has its own temperature measuring device, allowing the system to capture spatial temperature variations and calculate a more accurate average temperature that reflects the actual thermal state of the ceiling.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The temperature measurement transitions from a single-point measurement to a multi-dimensional approach by measuring at multiple azimuthal positions around the central axis. This dimensional expansion allows the system to capture radial temperature distribution and compute a comprehensive average, significantly improving measurement accuracy.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Ease of manufacture

If the gap height between the process chamber ceiling and heat dissipation body varies locally due to tolerances or distortions, then the system is easier to manufacture, but the temperature uniformity across the process chamber ceiling deteriorates

Engineering Contradiction:
Improvegap space assembly easeVSAvoidtemperature uniformity precision
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The system compensates for gap height variations by dynamically adjusting the composition of the purge gas mixture. By changing the mixing ratio of gases with different thermal conductivities, the system can modulate the thermal resistance of the purge gas to counteract the effects of local gap height variations, thereby maintaining uniform temperature distribution across the process chamber ceiling.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The system employs feedback control by continuously monitoring temperatures at multiple azimuthal positions and using these measurements to adjust the purge gas composition. The average temperature and temperature differences guide the adjustment of gas mixing ratios, creating a closed-loop control system that maintains temperature uniformity despite manufacturing tolerances.

Inventive Principle:
Principle #23Feedback

3Ease of operation

If the purge gas composition is adjusted based on arbitrary temperature signals, then the temperature control response is simple, but the average surface temperature deviates from the setpoint value

Engineering Contradiction:
Improvepurge gas adjustment easeVSAvoidtemperature setpoint accuracy
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The system uses feedback control by continuously monitoring temperatures at multiple azimuthal positions and using these measurements to adjust the purge gas composition. The average temperature and temperature differences guide the adjustment of gas mixing ratios, creating a closed-loop control system that maintains temperature uniformity despite manufacturing tolerances.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The system compensates for gap height variations by dynamically adjusting the composition of the purge gas mixture. By changing the mixing ratio of gases with different thermal conductivities, the system can modulate the thermal resistance of the purge gas to counteract the effects of local gap height variations, thereby maintaining uniform temperature distribution across the process chamber ceiling.

Inventive Principle:
Principle #35Parameter changes

4Ease of manufacture

If different gap heights exist at different locations, then the assembly is more tolerant to manufacturing variations, but the reaction rates become inconsistent leading to qualitatively different layer deposition

Engineering Contradiction:
Improvegap space assembly toleranceVSAvoidlayer deposition consistency
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The system compensates for gap height variations by dynamically adjusting the composition of the purge gas mixture. By changing the mixing ratio of gases with different thermal conductivities, the system can modulate the thermal resistance of the purge gas to counteract the effects of local gap height variations, thereby maintaining uniform temperature distribution across the process chamber ceiling.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The system applies local quality control by independently addressing temperature variations at different azimuthal positions. Through multi-point temperature measurement and targeted adjustment of purge gas composition, the system ensures that each region of the process chamber ceiling maintains the appropriate temperature for consistent layer deposition, even when gap heights vary locally.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach ensures a more uniform temperature distribution across the process chamber ceiling, enhancing the energy balance and consistency of layer deposition on substrates, thereby improving the quality of deposited layers.

Implementation Method 1

heat is transported from the susceptor, through a process chamber, to a process chamber ceiling

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 2

through the process chamber ceiling, and from the process chamber ceiling, through a gap space, to a heat dissipation body

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 3

The purge gas consists of a mixture of at least two gases, which differ greatly with regard to their thermal conductivity properties, so that, depending on the mixing ratio of the two gases, either a highly thermally conductive purge gas, or an only slightly thermally conductive purge gas, is flowing through, or is present in, the gap space

Methodology Applied
Scientific EffectThermal conduction through gas: Conduction (thermal)

Implementation Method 4

a temperature of the process chamber ceiling is measured by means of at least two sensors, in each case at different azimuthal angular positions

Methodology Applied
Scientific EffectThermal radiation: Thermal Radiation

Data Source

PatentUS11713505B2Device and method for controlling the ceiling temperature of a CVD reactor
Publication Date: 2023.08.01 AIXTRON AG
  • US11713505B2 patent drawing
  • US11713505B2 patent drawing
  • US11713505B2 patent drawing

AI summary

A CVD reactor may include a susceptor, process chamber and heat dissipation body. In the CVD reactor, one or more layers can be deposited on one or more substrates. The susceptor is heated by a heating devices. Heat is transported from susceptor, through a process chamber towards the process chamber ceiling, through the process chamber ceiling, and from the process chamber ceiling through a gap space to the heat dissipation body. The temperature of the process chamber ceiling is measured at at least two different azimuth angle positions about a central axis of the process chamber. The radial distance of the respective measurement points or zones from the central axis of the process chamber may be equal to one another. The at least two temperature measurement values are used to produce an average value or a difference value.